Pore compaction and crack evolution of shale rock under high-speed impact loading and different confining pressures

被引:0
|
作者
Wang, Jiawei [1 ]
Zhu, Chuanjie [1 ]
Ma, Cong [1 ]
Liang, Zhongqiu [2 ]
Li, Ke [1 ]
Zhai, Cheng [1 ]
Lin, Baiquan [1 ]
机构
[1] China Univ Min & Technol, Fac Safety Engn, Xuzhou 221116, Jiangsu, Peoples R China
[2] CCTEG Shenyang Res Inst, Shenyang 113122, Liaoning, Peoples R China
来源
SCIENTIFIC REPORTS | 2025年 / 15卷 / 01期
基金
中国国家自然科学基金;
关键词
Shale; SHPB; Confining pressure; Pore compaction; Crack extension; MERCURY INTRUSION POROSIMETRY; ORGANIC-RICH SHALE; FRACTURE-TOUGHNESS; YANGTZE PLATFORM; SICHUAN BASIN; GAS; STRENGTH; CHINA; ADSORPTION; MECHANISM;
D O I
10.1038/s41598-025-90347-y
中图分类号
O [数理科学和化学]; P [天文学、地球科学]; Q [生物科学]; N [自然科学总论];
学科分类号
07 ; 0710 ; 09 ;
摘要
High-speed impact loading has a crucial effect on pore compaction and microscopic crack evolution for shale at different confining pressure (P-c). In this study, we selected the shales from Jiangxi (JX) and Sichuan Province (SC) in China, and then performed Split Hopkinson pressure bar (SHPB) experiments at P-c = 0, 5, 15, and 25 MPa. Further, the impacted shales were tested by low temperature nitrogen adsorption (LTNA), mercury intrusion porosimetry (MIP) and environmental scanning electron microscope (ESEM). The results showed that confining pressure could cause different degrees of pore compaction and crack blockage: total pore volume (TPV) based on MIP of the JX and SC shales at different confining pressures decreased by 24.3 similar to 69.2% and 54.1 similar to 66.5%, respectively; total pore volume based on LTNA decreased by 36.2 similar to 49.0% and 49.9 similar to 58.2%, respectively; total specific surface area (TSSA) based on BET model decreased 68.3 similar to 75.8% and 39.5 similar to 60.0%, respectively. It was found that the confining pressure had a more significant effect on macropores relative to mesopores. Confining pressure also changed the failure patterns of shales. The shales at low confining pressure (P-c = 0, 5, and 15 MPa) showed a marked characteristic of brittle shear damage. However, the shales at high confining pressure (P-c = 25 MPa) showed a brittle-ductile transition (BDT) phenomenon. Additionally, high confining pressure resulted in a tiny ductile damage and a significant increase in elastic modulus. Besides, the effect of different mineral compositions and grain sizes on crack extension was discussed. This study is meaningful for understanding and controlling pore compaction and crack extension, thus improving production processes of dynamic shale gas production technology.
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页数:20
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