Cermet coatings obtained by electric spark alloying to increase service life of dental instruments

被引:0
|
作者
Gvetadze, R. [1 ]
Arutyunov, S. [1 ]
Kryuchkov, S. [2 ]
Antipov, M. [3 ]
Bazhin, P. [3 ,4 ]
Mustafaev, M. [5 ]
Deshev, A. [5 ]
Tsarev, V. [1 ]
Andreev, M. [1 ]
Katkov, I. [1 ]
Agasieva, S. [4 ]
Avdeeva, V. [6 ]
机构
[1] Russian Univ Med, Dolgorukovskaya Str 4, Moscow 127006, Russia
[2] LLC Profident Grp, Solnechnaya St 6, Zhukovskii 140180, Moscow Region, Russia
[3] Russian Acad Sci, Merzhanov Inst Struct Macrokinet & Mat Sci, Akademika Osipyana Str 8, Chernogolovka 142432, Moscow Region, Russia
[4] RUDN Univ, Dept Nanotechnol & Microsyst Technol, Miklukho Maklaya Str 6, Moscow 117198, Russia
[5] Kabardino Balkarian State Univ, Chernyshevsky Str 173, Nalchik 360004, Russia
[6] Kurnakov Inst Gen & Inorgan Chem, Russian Acad Sci, Moscow 119991, Russia
关键词
Cermet; Protective coating; SHS; Electrode; Electro spark alloying; Corrosion; Dentistry; CORROSION-RESISTANCE; TITANIUM; INACTIVATION; PATHOGENS; PRODUCTS; BEHAVIOR; RODS;
D O I
10.1016/j.ceramint.2024.10.112
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
The article presents the results of our study of protective cermet coatings obtained by the method of electric spark alloying on a dental instrument (excavator) using SHS (self-propagating high-temperature synthesis) electrodes based on TiC-NiCr. The influence of discharge energy during electric spark alloying on the roughness, thickness, and proportion of the TiC carbide phase in the cermet coating has been established. It has been shown that during electric spark alloying, the material of the used SHS electrode and the surface of the substrate melt, their convective mixing occurs, and during crystallization, coatings are formed that consist of a strengthening phase TiC and iron-based solid solutions: Fe9.64Ti0.36, F1.88C0.12, and Cr-Ni-Fe-C. It has been found that the maximum size of TiC grains is formed on the surface of the cermet coating, and as they approach the substrate, their size decreases to less than 10 nm. It has been found that the microhardness of the surface of the resulting cermet coatings increased to 6.2 times compared to the microhardness of the original metal base, which was 2 GPa. The results of scanning electron microscopy and energy dispersive analysis of the surface of samples with and without cermet coating before and after corrosion tests are presented. The influence of disinfectants (2 and 100 % Trilox, Wendelin, MegaDes-ortho) on the corrosion resistance of samples with and without developed protective cermet coatings at room and elevated temperatures up to 50 degrees C and their exposure for 120 h has been established.
引用
收藏
页码:52613 / 52621
页数:9
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