A rapid gas-chromatographic method for determining organochlorine insecticides in water media

被引:0
|
作者
Galaktionova, M.A. [1 ]
Nevinnaya, L.V. [1 ]
机构
[1] Inst Kolloidnoj Khimii i Khimii Vody, AN UkrSSR, Kiev, Russia
来源
Khimiya i Tekhnologiya Vody | 1991年 / 13卷 / 11期
关键词
Chlorine Compounds - Chemical Analysis - Pesticides - Analysis - Solutions - Concentration - Water Analysis - Optimization;
D O I
暂无
中图分类号
学科分类号
摘要
A rapid gas-chromatographic method is suggested to determine isomers of hexachlorocyclohexane (HCCH), DDT, and its analogs for the control of experiments on insecticide adsorption by activated carbon. The method permits decreasing the volume of the analyzed sample, as compared to the known procedures, to 40-100 ml, excluding the drying stage of the hexane extract and the evaporation stage when determining HCCH. The detection limits for α-, β-, γ-HCCH and DDT are 0.01; 0.1; 0.025 and 0.1 ng respectively. The duration of analysis is 15-30 min, the error does not exceed 3-5%.
引用
收藏
页码:987 / 991
相关论文
共 50 条
  • [31] DETERMINATION OF NIFEDIPINE IN PLASMA BY A RAPID CAPILLARY GAS-CHROMATOGRAPHIC METHOD
    LEGUELLEC, C
    BUN, H
    GIOCANTI, M
    DURAND, A
    BIOMEDICAL CHROMATOGRAPHY, 1992, 6 (01) : 20 - 23
  • [32] RAPID GAS-CHROMATOGRAPHIC METHOD FOR THE QUANTITATION OF PHYTANIC ACID IN SERUM
    JACOB, K
    VOGT, W
    KNEDEL, M
    JOURNAL OF CLINICAL CHEMISTRY AND CLINICAL BIOCHEMISTRY, 1981, 19 (04): : 224 - 224
  • [33] RAPID GAS-CHROMATOGRAPHIC METHOD FOR QUANTITATION OF ETHCHLORVYNOL (PLACIDYL) IN SERUM
    EVENSON, MA
    POQUETTE, MA
    CLINICAL CHEMISTRY, 1974, 20 (02) : 212 - 216
  • [34] A RAPID GAS-CHROMATOGRAPHIC METHOD FOR THE QUANTITATION OF FLECAINIDE IN SERUM OR PLASMA
    BROWN, PI
    RABKIN, M
    CLINICAL CHEMISTRY, 1987, 33 (06) : 1016 - 1016
  • [35] SIMULTANEOUS GAS-CHROMATOGRAPHIC DETERMINATION OF 4 ORGANOPHOSPHORUS INSECTICIDES
    ZORAKU, M
    OKURA, Y
    BUNSEKI KAGAKU, 1976, 25 (11) : 790 - 794
  • [36] GAS-CHROMATOGRAPHIC METHOD FOR DETERMINING CHLORIDE AND BROMINE IONS IN AQUEOUS SOLUTION
    BERGMANN, JG
    MARTIN, RL
    ANALYTICAL CHEMISTRY, 1962, 34 (08) : 911 - &
  • [37] DIRECT GAS-CHROMATOGRAPHIC METHOD FOR DETERMINING THE HOMOLOG COMPOSITION OF BENZALKONIUM CHLORIDES
    NG, LK
    HUPE, M
    HARRIS, AG
    JOURNAL OF CHROMATOGRAPHY, 1986, 351 (03): : 554 - 559
  • [38] RAPID GAS-CHROMATOGRAPHIC ANALYSIS ON SPHEROSIL
    CIRENDINI, S
    VERMONT, J
    GRESSIN, JC
    GUILLEMI.CL
    JOURNAL OF CHROMATOGRAPHY, 1973, 84 (01): : 21 - 36
  • [39] Iteration method for determining an adsorption isotherm from gas-chromatographic data
    Shkilev, VP
    Bogillo, VI
    ZHURNAL FIZICHESKOI KHIMII, 1998, 72 (09): : 1662 - 1666
  • [40] GAS-CHROMATOGRAPHIC METHOD FOR DETERMINING FREE FATTY-ACIDS IN CHEESE
    MARTINHERNANDEZ, MC
    ALONSO, L
    JUAREZ, M
    FONTECHA, J
    CHROMATOGRAPHIA, 1988, 25 (02) : 87 - 90