Technological parameters in the synthesis of 1,1,1-trichloroethane from vinylidene chloride

被引：0
|
作者：
Milchert, Eugeniusz [1 ]
Goc, Waldemar [1 ]
Stefanska, Jolanta [1 ]
Pazdzioch, Waldemar [1 ]
机构：
[1] Technical Univ of Szczecin, Szczecin, Poland
来源：
Industrial and Engineering Chemistry Research | 1996年 / 35卷 / 10期
关键词：
Catalysts - Chemical reactions - Composition - Ethane - Hydrogen inorganic compounds - Modification - Raw materials - Solvents - Temperature - Thermodynamic properties - Vinyl resins;
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学科分类号：
摘要：
The optimum parameters in the synthesis of 1,1,1-trichloroethane during the reaction between vinylidene chloride and hydrogen chloride are as follows: temperature, 22°C; catalyst (FeCl3) concentration, 0.3% by weight;, equimolar ratio of raw materials; VDC flow rate, 0.22-0.23 cm3 cm-3 h-1. Changing these parameters does not result in considerable change in the product yield.
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页码：3290 / 3294
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