Reactions with hydrazonoyl halides. XXVIII: Synthesis of some 2-thiazolylimino-2,3-dihydro-1,3,4-thiadiazoles

被引:0
|
作者
Abdelhamid, Abdou O. [1 ]
Abdel-Riheem, Nadia A. [1 ]
Hassan, Nabil M. [1 ]
机构
[1] Department of Chemistry, Faculty of Science, Cairo University, Giza 12613, Egypt
关键词
Hydrazonoyl halides - Thiazolylimino dihydro thiadiazoles;
D O I
暂无
中图分类号
学科分类号
摘要
The structures of the hydrazonyl halides, thiadiazoles, and nitrilium amide 9 were elucidated on the basis of elemental analyses, spectral data, and alternative methods of synthesis. The infrared spectroscopic analysis revealed the absence of any bands at 1200 cm- attributable to a C = S group. The melting points of the compound were determined by an electrothermal apparatus.
引用
收藏
相关论文
共 50 条
  • [21] Susceptibility of 2-arylidene-3,5.diaryl-2,3-dihydro-1,3,4-thiadiazoles to hydrolysis
    Mueller, JL
    Gottardo, C
    Jones, TRB
    Gibson, MS
    PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS, 1998, 132 : 163 - 166
  • [22] Reaction of hydrazonoyl halides 55: Synthesis of 2,3-dihydro[1,3,4]-thiadiazoles containing steroid moiety
    Abdelhamid, A. O.
    Baghos, V. B.
    Doss, S. H.
    Halim, M. M. A.
    PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS, 2007, 182 (12) : 2843 - 2854
  • [23] Reactions with hydrazonoyl halides 38: Synthesis of pyrrolo[3,4-c]pyrazoles, pyrazoles and 1,3,4-thiadiazoles
    Abdelhamid, AO
    Abdel-Wahab, BAM
    AFINIDAD, 2004, 61 (509) : 65 - 73
  • [24] STUDY ON 2,3-DIHYDRO-1,3,4-THIADIAZOLES AS THE CONDENSATION PRODUCTS OF THIOBENZOYL HYDRAZIDE WITH CARBONYL-COMPOUNDS
    ZELENIN, KN
    KHRUSTALEV, VA
    PINSON, VV
    ALEKSEEV, VV
    ZHURNAL ORGANICHESKOI KHIMII, 1980, 16 (10): : 2237 - 2238
  • [25] Synthesis of 2-polyfluoroalkyl-2,3-dihydro-1,3,4-thiadiazoles via regioselective [3+2] cycloaddition of nitrile imines to polyfluoroalkanethioamides
    Sergiy S. Mykhaylychenko
    Nadezhda V. Pikun
    Eduard B. Rusanov
    Alexander B. Rozhenko
    Yuriy G. Shermolovich
    Chemistry of Heterocyclic Compounds, 2017, 53 : 1268 - 1276
  • [26] Synthesis of 2-polyfluoroalkyl-2,3-dihydro-1,3,4-thiadiazoles via regioselective [3+2] cycloaddition of nitrile imines to polyfluoroalkanethioamides
    Mykhaylychenko, Sergiy S.
    Pikun, Nadezhda V.
    Rusanov, Eduard B.
    Rozhenko, Alexander B.
    Shermolovich, Yuriy G.
    CHEMISTRY OF HETEROCYCLIC COMPOUNDS, 2017, 53 (11) : 1268 - 1276
  • [27] Reactions with hydrazonoyl halides XXII: Synthesis of pyrrolo[3,4-C]pyrzoline, pyrazoline, pyrazole, and 2,3-dihydro-1,3,4-thiadiazole derivatives
    Abdelhamid, AO
    Abed, NM
    Al-Fayez, FZ
    PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS, 2000, 156 : 35 - 52
  • [28] Reactions of hydrazonoyl halides 37:: Synthesis of triazolo[4,3-a]pyrimidines, 1,3,4-thiadiazoles and 1,3,4-selenadiazoles
    Abdelhamid, AO
    Abdel-Wahab, BAM
    Al-Atoom, AA
    PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS, 2004, 179 (03) : 601 - 613
  • [29] Eco-Friendly Synthesis of 3-Aryl-2,3-dihydro-1,3,4-thiadiazoles Based on Benzofuran and Chromone Moieties
    Abdel-Aziem, Anhar
    El-Sawy, Eslam R.
    Kirsch, Gilbert
    POLYCYCLIC AROMATIC COMPOUNDS, 2022, 42 (05) : 2617 - 2631
  • [30] Anti-proliferative 2,3-dihydro-1,3,4-thiadiazoles targeting VEGFR-2: Design, synthesis, in vitro, , and in silico studies
    Elkady, Hazem
    Elgammal, Walid E.
    Mahdy, Hazem A.
    Zara, Susi
    Carradori, Simone
    Husein, Dalal Z.
    Alsfouk, Aisha A.
    Ibrahim, Ibrahim M.
    Elkaeed, Eslam B.
    Metwaly, Ahmed M.
    Eissa, Ibrahim H.
    COMPUTATIONAL BIOLOGY AND CHEMISTRY, 2024, 113