Preparation of β-SiC nanostructured powder by sol-gel process

被引:0
|
作者
Zhang, Hongtao [1 ]
Xu, Zhongyang [1 ]
Xu, Hui [1 ]
机构
[1] Hubei Inst of Technology, Wuhan, China
来源
关键词
Heat treatment - Hydrolysis - Nanostructured materials - Silicon carbide - Sol-gels;
D O I
暂无
中图分类号
学科分类号
摘要
The monodispersed spherical β-SiC nanostructured powder was synthesized by a sol-gel process derived from the hydrolysis of a mixture of two organisms. The gel powder become monodispersed spherical β-SiC nanostructured powder by heat treatment at 900-1300 °C in Ar atmosphere. The sizes of β-SiC powder of high purity and low oxygen are about 10 nm. The content of β-SiC is 99.92%. The morphology, structure and grain size were studied by XRD, TEM and Raman spectroscopy. The process of the growth mechanism of the β-SiC nanostructured powder at different temperatures was discussed.
引用
收藏
页码:366 / 368
相关论文
共 50 条
  • [1] Sol-gel preparation of nanostructured adsorbents
    Lin, YS
    Deng, SG
    ADSORPTION AND ITS APPLICATIONS IN INDUSTRY AND ENVIRONMENTAL PROTECTION, VOL I: APPLICATIONS IN INDUSTRY, 1999, 120 : 653 - 686
  • [2] Preparation of gallium nitride (GaN) powder by sol-gel process
    Liu Yian
    Xue Chengshan
    Zhuang Huizhao
    Zhang Xiaokai
    Tian Deheng
    Wu Yuxin
    Sun Lili
    Ai Yujie
    Wang Fuxue
    RARE METAL MATERIALS AND ENGINEERING, 2006, 35 : 378 - 380
  • [3] Effects of the preparation of SiC by sol-gel
    Xing, Su-Li
    Wang, Jun
    Zeng, Jing-Cheng
    Xiao, Jia-Yu
    Guofang Keji Daxue Xuebao/Journal of National University of Defense Technology, 2002, 24 (02):
  • [4] Sol-gel synthesis and characterization of nanostructured hydroxyapatite powder
    Kim, IS
    Kumta, PN
    MATERIALS SCIENCE AND ENGINEERING B-SOLID STATE MATERIALS FOR ADVANCED TECHNOLOGY, 2004, 111 (2-3): : 232 - 236
  • [5] Synthesis of SiC Nanoparticles by a Sol-Gel Process
    Jeong, Kwang-Jin
    Bae, Dong-Sik
    KOREAN JOURNAL OF MATERIALS RESEARCH, 2013, 23 (04): : 246 - 249
  • [6] Synthesis of SiC precursors by sol-gel process
    Tian, JM
    Li, JW
    Dong, LM
    JOURNAL OF INORGANIC MATERIALS, 1999, 14 (02) : 297 - 301
  • [7] Preparation and electrochemical properties of nanocrystalline NiO powder prepared by sol-gel process
    School of Materials Science and Engineering, Henan University of Science and Technology, Luoyang 471003, China
    不详
    Cailiao Rechuli Xuebao, 2008, 4 (39-42):
  • [8] Nanostructured optical fibre obtained by the sol-gel process
    Brasse, Gurvan
    Restoin, Christine
    Auguste, Jean-Louis
    Roy, Philippe
    Leparmentier, Stephanie
    Blondy, Jean-Marc
    PROCEEDINGS OF THE 1ST WSEAS INTERNATIONAL CONFERENCE ON RECENT ADVANCES IN NANOTECHNOLOGY, 2009, : 41 - 46
  • [9] Study on preparation and property of SiC ceramics by sol-gel
    Chen, Zhi-Lin
    Zhang, Jian
    Zhou, Jian-Bin
    Fu, Feng
    Gongneng Cailiao/Journal of Functional Materials, 2010, 41 (01): : 69 - 72
  • [10] Preparation of Insulating SiO2 Nanostructured Thin Films by the Sol-Gel Process
    Hsieh, Tung-Li
    Chu, Ann-Kuo
    Huang, Wen-Yao
    JOURNAL OF NANOSCIENCE AND NANOTECHNOLOGY, 2013, 13 (01) : 279 - 287