Ultrasonic evaluation of the sol-gel synthesis of silica glass

被引：0
|
作者：
Osaka Natl Research Inst, Osaka, Japan [1 ]
机构：
来源：
Ultrasonics | / 2-5卷 / 335-338期
关键词：
Acoustic wave velocity - Alcohols - Evaporation - Fused silica - Gelation - Hydrolysis - Monomers - Oligomers - Sol-gels - Solvents - Spectroscopic analysis - Synthesis (chemical);
D O I：
暂无
中图分类号：
学科分类号：
摘要：
The isothermal gelation process in silicon alkoxide solutions has been investigated using ultrasonic pulse spectroscopy. The process in alcoholic solutions of monomeric and oligomeric precursors was monitored continuously by changes in ultrasonic longitudinal wave velocity. Under a closed system, the velocity gradually decreased as the gelation advanced. However, in an open system, the velocity slightly increased before decreasing after gelation. In order to understand the cause of these changes in the velocity, the effects of hydrolysis and evaporation of the solvent were studied.
引用
收藏
相关论文
共 50 条
  • [21] Spinnability and crystallizability of silica glass fiber by the sol-gel method
    Xu, YD
    Zhou, WC
    Zhang, LT
    Cheng, LF
    JOURNAL OF MATERIALS PROCESSING TECHNOLOGY, 2000, 101 (1-3) : 44 - 46
  • [22] Viscosity of silica glass prepared from sol-gel powder
    Yamahara, K
    Shima, K
    Utsunomiya, A
    Tsurita, Y
    JOURNAL OF NON-CRYSTALLINE SOLIDS, 2004, 349 : 341 - 346
  • [23] The structure of a bioactive calcia-silica sol-gel glass
    Skipper, LJ
    Sowrey, FE
    Pickup, DM
    Drake, KO
    Smith, ME
    Saravanapavan, P
    Hench, LL
    Newport, RJ
    JOURNAL OF MATERIALS CHEMISTRY, 2005, 15 (24) : 2369 - 2374
  • [24] Silica antireflective films on glass produced by the sol-gel method
    Bautista, MC
    Morales, A
    SOLAR ENERGY MATERIALS AND SOLAR CELLS, 2003, 80 (02) : 217 - 225
  • [25] Porosity of sol-gel derived silica coatings on glass substrates
    Ayral, A
    El Mansouri, A
    Vieira, MP
    Pilon, C
    JOURNAL OF MATERIALS SCIENCE LETTERS, 1998, 17 (11) : 883 - 885
  • [26] Transparent Superhydrophobic silica coatings on glass by sol-gel method
    Mahadik, Satish A.
    Kavale, Mahendra S.
    Mukherjee, S. K.
    Rao, A. Venkateswara
    APPLIED SURFACE SCIENCE, 2010, 257 (02) : 333 - 339
  • [27] The luminescence of PbS nanoparticles embedded in sol-gel silica glass
    Yang, P
    Song, CF
    Lü, MK
    Yin, X
    Zhou, GJ
    Xu, D
    Yuan, DR
    CHEMICAL PHYSICS LETTERS, 2001, 345 (5-6) : 429 - 434
  • [28] Effect of the silica sol-gel coatings on the properties of glass substrate
    Nikolic, L
    Radonjic, L
    CERAMICS INTERNATIONAL, 1998, 24 (07) : 547 - 552
  • [29] REDUCTION OF CHLORINE CONTENT IN SOL-GEL DERIVED SILICA GLASS
    SUSA, K
    MATSUYAMA, I
    SATOH, S
    SUGANUMA, T
    JOURNAL OF NON-CRYSTALLINE SOLIDS, 1986, 79 (1-2) : 165 - 176
  • [30] Sol-gel synthesis of colloidal silica using cyclohexane
    Indian Assoc for the Cultivation of, Science, Calcutta, India
    J Mater Sci Lett, 21 (1872-1874):
12345