Studies on the Matrix Assisted Laser Desorption/Ionization Time of Flight Mass Spectrometry( I ) - Calixarene Compounds
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作者:
Xiong, Shao-Xiang
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Beijing Mass Spectrometry Center, Institute of Chemistry, Chinese Academy of Sciences, Beijing 100080, ChinaBeijing Mass Spectrometry Center, Institute of Chemistry, Chinese Academy of Sciences, Beijing 100080, China
Xiong, Shao-Xiang
[1
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Xin, Bin
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Beijing Mass Spectrometry Center, Institute of Chemistry, Chinese Academy of Sciences, Beijing 100080, ChinaBeijing Mass Spectrometry Center, Institute of Chemistry, Chinese Academy of Sciences, Beijing 100080, China
Xin, Bin
[1
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Wang, Guang-Hui
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Beijing Mass Spectrometry Center, Institute of Chemistry, Chinese Academy of Sciences, Beijing 100080, ChinaBeijing Mass Spectrometry Center, Institute of Chemistry, Chinese Academy of Sciences, Beijing 100080, China
Wang, Guang-Hui
[1
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Liu, Guo-Quan
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Beijing Mass Spectrometry Center, Institute of Chemistry, Chinese Academy of Sciences, Beijing 100080, ChinaBeijing Mass Spectrometry Center, Institute of Chemistry, Chinese Academy of Sciences, Beijing 100080, China
Liu, Guo-Quan
[1
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[1] Beijing Mass Spectrometry Center, Institute of Chemistry, Chinese Academy of Sciences, Beijing 100080, China
Matrix assisted laser desorption/ionization time of flight(MALDI-TOF) mass spectrometry was used for the mass spectrometry analyses of calixarene compounds. The influences of sample preparation, detection mode, laser intensity, voltage and time of delayed extraction on the measurement results were investigated. The mass spectrometry data of twenty-five compounds have shown the MALDI-TOF mass spectra with satisfactory performances in sensitivity, resolution and accuracy can be easily obtained. A new mass spectrometry method was established and provided for the mass identification of calixarene compounds.
机构:
Samsung Electromech Co Ltd, Analyt Res Grp, Suwon 443743, Gyeonggi, South KoreaSamsung Electromech Co Ltd, Analyt Res Grp, Suwon 443743, Gyeonggi, South Korea
Cho, Donghyun
Hong, Sangsu
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Samsung Electromech Co Ltd, Analyt Res Grp, Suwon 443743, Gyeonggi, South KoreaSamsung Electromech Co Ltd, Analyt Res Grp, Suwon 443743, Gyeonggi, South Korea
机构:
Faculty of Pharmaceutical Sciences, Toho University, Funabashi, Chiba, Japan
Faculty of Pharmaceutical Sciences, Toho University, 2-2-1 Miyama, Funabashi, Chiba 274-8510, JapanFaculty of Pharmaceutical Sciences, Toho University, Funabashi, Chiba, Japan
Fukai, Toshio
Kuroda, Jun
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Faculty of Pharmaceutical Sciences, Toho University, Funabashi, Chiba, JapanFaculty of Pharmaceutical Sciences, Toho University, Funabashi, Chiba, Japan
Kuroda, Jun
Nomura, Taro
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Faculty of Pharmaceutical Sciences, Toho University, Funabashi, Chiba, JapanFaculty of Pharmaceutical Sciences, Toho University, Funabashi, Chiba, Japan