Preparation and structure characterization of ordered cubic Zr-doped mesoporous silica by EISA method

被引：0

作者：

Chu, Bin ^{[1
]}

Wang, Run-Wei ^{[1
]}

Shen, Qi-Hui ^{[1
]}

Chen, Lu ^{[1
]}

Wan, Li-Feng ^{[1
]}

Zhu, Guang-Shan ^{[1
]}

Qiu, Shi-Lun ^{[1
]}

机构：

[1] State Key Laboratory of Inorganic Synthesis and Preparative Chemistry, Jilin University, Changchun 130012, China

来源：

Gaodeng Xuexiao Huaxue Xuebao/Chemical Journal of Chinese Universities | 2007年 / 28卷 / 08期

关键词：

D O I：

暂无

中图分类号：

学科分类号：

摘要：

Highly ordered cubic Zr-doped mesoporous silica was directly prepared with Evaporation-Induced Self Assembly method (EISA) with triblock copolymers (Pluronic PI 23) as the structure-directing agents. The mesoporous material was characterized via small-angle powder X-ray diffraction (XRD), transmission electron microscopy (TEM), and nitrogen adsorption. The results show that the product has a face-centered cubic structure with space group of Fd3m. N2 sorption revealed that the Zr-doped mesoporous silica has not only ordered structures, but also high surface area (550 m2/g), large pore volume (0.66 cm3/g), as well as uniform pore size (4.0 nm).

引用

页码：1428 / 1430

共 50 条

[21] Structure Fingerprints of Ordered Mesoporous Silica
Fantini, Marcia C. A.
Silva, Luis
Matos, Jivaldo
Mercuri, Lucildes
ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES, 2005, 61 : C404 - C404
[22] Preparation, structural and optical characterization of rare earth doped mesoporous Y2O3 thin films by EISA method
Castro, Yolanda
Julian-Lopez, Beatriz
Boissiere, Cedric
Viana, Bruno
Grosso, David
Sanchez, Clement
MICROPOROUS AND MESOPOROUS MATERIALS, 2007, 103 (1-3) : 273 - 279
[23] Preparation and characterization of structurally stable hexagonal and cubic mesoporous silica thin films
Jung, JI
Bae, JY
Bae, BS
JOURNAL OF SOL-GEL SCIENCE AND TECHNOLOGY, 2004, 31 (1-3) : 179 - 183
[24] Preparation and Characterization of Structurally Stable Hexagonal and Cubic Mesoporous Silica Thin Films
Ji-In Jung
Jae Young Bae
Byeong-Soo Bae
Journal of Sol-Gel Science and Technology, 2004, 31 : 179 - 183
[25] Preparation, characterization and electrical conduction mechanism of polyaniline/ordered mesoporous silica composites
Santos Pedroso, Cassio Cardoso
Junqueira, Vania
Lacerda Rubinger, Carla Patricia
Martins, Tereza Silva
Faez, Roselena
SYNTHETIC METALS, 2013, 170 : 11 - 18
[26] Preparation and characterization of ordered mesoporous La2Zr2O7
Liu, Ruiping
Su, Weiming
Wang, Chang-An
Zhao, Huiyou
Kuei Suan Jen Hsueh Pao/Journal of the Chinese Ceramic Society, 2015, 43 (06): : 794 - 797
[27] Preparation of ordered iron nanowires in the mesoporous silica matrix
Napol'skij, K.S.
Kolesnik, I.V.
Eliseev, A.A.
Lukashin, A.V.
Vertegel', A.A.
Tret'yakov, Yu.D.
Doklady Akademii Nauk, 2002, 386 (02) : 207 - 211
[28] Synthesis of Ordered Cubic Periodic Mesoporous Silica with High Hydrothermal Stability
Lai Xiao-yong
Tu Jin-chun
Wang Hong
Du Jiang
Yang Mei
Mao Dan
Xing Chao-jian
Wang Dan
Li Xiao-tian
CHEMICAL RESEARCH IN CHINESE UNIVERSITIES, 2009, 25 (05) : 773 - 774
[29] Robust Mg(Ca)Zr-Doped Acid-Base Bifunctional Mesoporous Silica and Their Applications in the Deacetalization-Knoevenagel Reaction
Cai, Menglu
Wang, Xiaozhong
Fang, Yangyang
Chen, Yingqi
Dai, Liyan
INORGANIC CHEMISTRY, 2021, 60 (12) : 8924 - 8935
[30] Synthesis of Ordered Cubic Periodic Mesoporous Silica with High Hydrothermal Stability
LAI Xiao-yong1
2. State Key Laboratory of Multi-phase Complex System
Chemical Research in Chinese Universities, 2009, 25 (05) : 773 - 774

← 1 2 3 4 5 →