Preparation and characterization of copper oxide nanoparticles through solid state thermal decomposition of an aqua nitrato copper(II) complex with a tridentate schiff-base ligand as a new precursor

被引：0
|
作者：
Monadi N. [1 ]
Saeednia S. [2 ]
Iranmanesh P. [3 ]
Ardakani M.H. [2 ]
Sinaei S. [2 ]
机构：
[1] Department of Inorganic Chemistry, Faculty of Chemistry, University of Mazandaran, Babolsar
[2] Department of Chemistry, Faculty of Science, Vali-e-Asr University of Rafsanjan, Rafsanjan
[3] Department of Physics, Faculty of Science, Vali-e-Asr University of Rafsanjan, Rafsanjan
来源：
Nanoscience and Nanotechnology - Asia | 2019年 / 9卷 / 01期
关键词：
Copper complex; Copper(II) oxide; Nanostructures; Schiff-base ligand; Solvothermal process; Sonochemistry;
D O I：
10.2174/2210681207666170703160109
中图分类号：
学科分类号：
摘要：
Introduction: In this study the synthesis and characterization of copper oxide nanoparticles via solid state thermal decomposition of a recently synthesized aqua nitrato copper(II) complex with a tridentate Schiff-base ligand (1) as a new precursor are reported. Materials & Methods: The copper complexes were obtained by sonochemical and solvothermal process and characterized by Scanning Electron Microscopy (SEM), X-ray powder Diffraction (XRD) and FT-IR spectroscopy. The thermal stability of compound (1) was studied by Thermogravimetric Analysis (TGA). The amount of initial reagents and the role of reaction time on size and morphology of nanostructure compound (1) were studied. CuO nanoparticles were simply synthesized at 500 o C under air atmosphere. Results & Conclusion: The diameter of CuO nanoparticles was estimated to be about 200 and 30 nm from copper complex precursor obtained by sonochemical and solvothermal methods respectively. © 2019 Bentham Science Publishers.
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页码：92 / 100
页数：8
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