2-Hydroxy-N'-(5-hydroxy-2-nitrobenzylidene)-3-methylbenzohydrazide

被引：1

作者：

Zhu, Zhao-Fu ^{[1
]}

Shao, Li-Juen ^{[1
]}

Shen, Xi-Hai ^{[1
]}

机构：

[1] Hebei Normal Univ Sci & Technol, Dept Chem, Qinhuangdao 066600, Peoples R China

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2012年 / 68卷

关键词：

data-to-parameter ratio = 13.7; mean σ(C-C) = 0.003 Å; R factor = 0.051; single-crystal X-ray study; T = 298 K; wR factor = 0.132;

D O I：

10.1107/S1600536812002437

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

The title compound, C 15H 13N 3O 5, was prepared by condensing 5-hydroxy-2-nitrobenzaldehyde and 2-hydroxy-3-methylbenzohydrazide in methanol. The two benzene rings make a dihedral angle of 3.9 (3)°. An intra-molecular O - H⋯O hydrogen bond is observed. The crystal structure is stabilized by intermolecular O - H⋯O and N - H⋯O hydrogen bonds, and C - H⋯O and π-π inter-actions [centroid-centroid distances = 3.5658 (17)-3.9287 (19) Å].

引用

页码：O559 / U1099

页数：8

共 50 条

[21] N′-(2-hydroxy-5-nitrobenzylidene)benzenesulfonohydrazide
Yusnita, Juahir
Ali, Hapipah M.
Puvaneswary, Subramaniam
Robinson, Ward T.
Ng, Seik Weng
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2008, 64 : O1583 - U3103
[22] 2-Hydroxy-N′-[(E)-(3-hydroxy-2-naphthyl)methylene]benzohydrazide
Sun, Yuying
Li, Hong-Gang
Wang, Xiao
Fu, Shizhou
Wang, Daqi
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : O262 - U1613
[23] (E)-N′-(5-Bromo-2-hydroxybenzylidene)-3-methylbenzohydrazide
Guo, Hai-Chang
Liu, Shi-Yong
Wang, Xiao-Ling
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O1878 - U1563
[24] N′-(2-Chlorobenzylidene)-2-hydroxy-3-methylbenzohydrazide
Han, You-Yue
Zhao, Qiu-Rong
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : O1025 - U1368
[25] (E)-2-Hydroxy-N′-(3-hydroxy-4-methoxybenzylidene)benzohydrazide
Luo, Zhi-Gang
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2007, 63 : O3672 - U1808
[26] N′-(2,4-Dichlorobenzylidene)-2-hydroxy-3-methylbenzohydrazide
Han, You-Yue
Zhao, Qiu-Rong
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : O1048 - U1557
[27] N′-(2,5-Dihydroxybenzylidene)-2-hydroxy-3-methylbenzohydrazide
Han, You-Yue
Li, Yong-Hong
Zhao, Qiu-Rong
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : O1091 - U219
[28] N′-(2,3-Dimethoxybenzylidene)-2-hydroxy-3-methylbenzohydrazide
Han, You-Yue
Zhao, Qiu-Rong
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : O1026 - U1377
[29] (E)-2-Hydroxy-N′-(2 naphthylmethylene)-benzohydrazide
Qiu, Xiao-Yang
Luo, Zhi-Gang
Yang, Sen-Lin
Liu, Wei-Sheng
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2006, 62 : O3531 - O3532
[30] 2-hydroxy-N′-(2-methoxynaphthylidene)benzohydrazide
Qiu, Xiao-Yang
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2008, 64 : O1829 - U2589

← 1 2 3 4 5 →