METHOD FOR ANALYSIS OF METHYL-BROMIDE RESIDUE IN CROPS

被引：0
|
作者：
ASAKA, S
SEGUCHI, K
机构：
来源：
JOURNAL OF PESTICIDE SCIENCE | 1979年 / 4卷 / 04期
关键词：
D O I：
暂无
中图分类号：
Q96 [昆虫学];
学科分类号：
摘要：
Methyl bromide liberated by modified Malone''s sweep codistillation method or acid reflux method was converted to N-methyl phthalimide with sodium hydroxide and phthalimide in N,N-dimethylformamide. This derivative was determined by a gas chromatograph equipped with an electron capture detector (ECD). Recoveries were 81-91% from wheat, hay, lettuce, tomato and carrot fortified at 0.125-0.05 ppm, with the detection limit of 0.0006-0.003 ppm.
引用
收藏
页码：453 / 456
页数：4
相关论文
共 50 条
  • [41] INVESTIGATIONS ON FUMIGATION OF WALNUTS WITH METHYL-BROMIDE
    SRINATH, D
    RAMCHANDANI, NP
    JOURNAL OF FOOD SCIENCE AND TECHNOLOGY-MYSORE, 1978, 15 (05): : 192 - 194
  • [42] DEGRADATION OF METHYL-BROMIDE IN ANAEROBIC SEDIMENTS
    OREMLAND, RS
    MILLER, LG
    STROHMALER, FE
    ENVIRONMENTAL SCIENCE & TECHNOLOGY, 1994, 28 (03) : 514 - 520
  • [43] EFFICIENCY OF RESPIRATOR CANISTERS WITH METHYL-BROMIDE
    TANAKA, S
    ABUKU, S
    IMAIZUMI, K
    ISHIZUKA, H
    SEKI, Y
    IMAMIYA, S
    INDUSTRIAL HEALTH, 1989, 27 (03) : 111 - 120
  • [44] BEHAVIOR OF METHYL-BROMIDE (TERABOL) IN SOIL
    LEPSCHY, J
    STARK, H
    SUSS, A
    GARTENBAUWISSENSCHAFT, 1979, 44 (02): : 84 - 89
  • [45] TRANSPORT AND TRANSFORMATION OF METHYL-BROMIDE IN SOILS
    BROWN, BD
    ROLSTON, DE
    SOIL SCIENCE, 1980, 130 (02) : 68 - 75
  • [46] PHOTODISSOCIATION OF METHYL-CHLORIDE AND METHYL-BROMIDE IN ATMOSPHERE
    ROBBINS, DE
    GEOPHYSICAL RESEARCH LETTERS, 1976, 3 (04) : 213 - 216
  • [47] EXPOSURE TO INORGANIC BROMIDES FROM GREENHOUSE CROPS WHERE METHYL-BROMIDE WAS APPLIED FOR SOIL FUMIGATION
    FALLICO, R
    FERRANTE, M
    ZENTRALBLATT FUR HYGIENE UND UMWELTMEDIZIN, 1991, 191 (5-6): : 555 - 562
  • [48] FACTORS INFLUENCING LETTUCE AND TOMATO BROMIDE UPTAKE AFTER METHYL-BROMIDE SOIL-DISINFESTATION .1. SOIL BROMIDE RESIDUE
    BLEYAERT, P
    DEJONCKHEERE, W
    REVUE DE L AGRICULTURE, 1988, 41 (01): : 63 - 78
  • [49] PLANT UPTAKE OF BROMIDE FOLLOWING SOIL FUMIGATION WITH METHYL-BROMIDE
    BROWN, AL
    BURAU, RG
    MEYER, RD
    RASKI, DJ
    WILHELM, S
    QUICK, J
    CALIFORNIA AGRICULTURE, 1979, 33 (04) : 11 - 13
  • [50] ORGANIC AND INORGANIC BROMIDE RESIDUES IN SPICES FUMIGATED WITH METHYL-BROMIDE
    REEVES, RG
    MCDANIEL, CA
    FORD, JH
    JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 1985, 33 (05) : 780 - 783
12345