A NEW BICYCLIC TIN SELENIUM COMPOUND - SYNTHESIS AND CRYSTAL-STRUCTURE OF [(CP(CO)2FE)3CLSN3SE4]

被引：0
|
作者：
MERZWEILER, K
KRAUS, H
机构：
来源：
ZEITSCHRIFT FUR NATURFORSCHUNG SECTION B-A JOURNAL OF CHEMICAL SCIENCES | 1993年 / 48卷 / 07期
关键词：
D O I：
暂无
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
[{CP(CO)2Fe}SnCl3] reacts with Na2Se in THF to form the compound [{CP(CO)2Fe}3ClSn3Se4] 1. 1 crystallizes in the monoclinic space group P2(1)/n with 4 formula units per unit cell. The lattice constants are a = 1435.2(7), b = 1124.4(4), c = 1972.7(12) pm, beta = 94.59(4)-degrees. According to the X-ray structure determination 1 contains a bicyclic Sn3Se4 framework.
引用
收藏
页码：1009 / 1012
页数：4
相关论文
共 50 条
  • [31] CC-LINKAGES OF ETHENE WITH CO2 ON AN IRON(0) COMPLEX SYNTHESIS AND CRYSTAL-STRUCTURE ANALYSIS OF [(PET3)2FE(C2H4)2]
    HOBERG, H
    JENNI, K
    ANGERMUND, K
    KRUGER, C
    ANGEWANDTE CHEMIE-INTERNATIONAL EDITION IN ENGLISH, 1987, 26 (02): : 153 - 155
  • [32] CRYSTAL-STRUCTURE OF TRANS-FE(CO)3[P(OCH3)3]2
    GINDEROW, D
    ACTA CRYSTALLOGRAPHICA SECTION B-STRUCTURAL SCIENCE, 1974, 30 (DEC15): : 2798 - 2802
  • [33] CRYSTAL-STRUCTURE OF THE COMPOUND CE2SC3SI4
    MOKRAYA, IR
    BODAK, OI
    GLADYSHEVSKY, EI
    KRISTALLOGRAFIYA, 1979, 24 (06): : 1274 - 1276
  • [34] CRYSTAL-STRUCTURE OF THE ZR2NB3GE4 COMPOUND
    SEROPEGIN, YD
    TABACHENKO, VV
    MYSKIV, MG
    KRISTALLOGRAFIYA, 1984, 29 (01): : 161 - 162
  • [35] SYNTHESIS AND X-RAY CRYSTAL-STRUCTURE OF HEXANUCLEAR COBALT-SELENIUM CLUSTER COMPOUND [CO6(MU-3-SE)8(PET3)6]BPH4
    HONG, MC
    LEI, XJ
    HUANG, ZY
    JIANG, FL
    LIU, HQ
    CHINESE SCIENCE BULLETIN, 1992, 37 (21): : 1798 - 1803
  • [36] SYNTHESIS OF (ME(3)SICH(2)SB)(N) AND REACTIONS WITH DITELLURIDES - CRYSTAL-STRUCTURE OF [CP(2)CO][ME(3)SICH(2)SBCL(3)]
    SILVESTRU, A
    BREUNIG, HJ
    EBERT, KH
    KALLER, R
    JOURNAL OF ORGANOMETALLIC CHEMISTRY, 1995, 501 (1-2) : 117 - 121
  • [37] Synthesis and structure of the cluster Fe2Mo2(μ3-Se)(μ3-AsMe)(μ3-Co)(μ-Co)(Co)5(η5-Cp)2
    S. N. Konchenko
    A. V. Virovets
    P. A. Petrov
    S. V. Tkachev
    Russian Chemical Bulletin, 1999, 48 : 988 - 990
  • [38] Synthesis and structure of the cluster Fe2Mo2(μ3-Se) (μ3-AsMe)(μ3-CO)(μ-CO)(CO)5(η5-Cp)2
    Konchenko, SN
    Virovets, AV
    Petrov, PA
    Tkachev, SV
    RUSSIAN CHEMICAL BULLETIN, 1999, 48 (05) : 988 - 990
  • [39] MEASUREMENT OF BARRIERS TO ARYL ROTATION IN CP(CO)2FE=CHC6H5+ AND CP(CO)2FE=CH(P-CH3C6H4)+
    BROOKHART, M
    TUCKER, JR
    HUSK, GR
    JOURNAL OF ORGANOMETALLIC CHEMISTRY, 1980, 193 (01) : C23 - C26
  • [40] SYNTHESIS AND CRYSTAL-STRUCTURE OF A 4-METAL KETENYLIDENE - [PPN]2[FE3CUI(CO)9(CCO)]
    GUNALE, AS
    JENSEN, MP
    STERN, CL
    SHRIVER, DF
    JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1991, 113 (04) : 1458 - 1460
12345