Synthesis of 6-carbomethoxy-3-Phenyl-5-(4-dimethylaminophenyl)-cyclohexenone

被引：0
|
作者：
Lobo, Gricela M. [1 ]
Charris, Jaime E. [1 ]
机构：
[1] Univ Cent Venezuela, Fac Farm, Lab Sintesis Organ, Caracas 1051, Venezuela
来源：
MOLBANK | 2005年 / 06期
关键词：
D O I：
10.3390/M452
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
A mixture of 4-dimethylaminochalcone 1 (0.25 g, 1.00 mmol), methyl acetoacetate (0.17 g, 1.5 mmol) in methanol (5.00 mL) and sodium metoxide (0.25 mg) was stirred at room temperature for 24 hour to give a yellow precipitate. Then it was filtered and washed with water. Recrystalized of the crude substance from methanol afforded pure cyclohexenone 2 (2.27 g, 97.00 %). © 2005 MDPI. All rights reserved.
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