Synthesis of 6-carbomethoxy-3-Phenyl-5-(4-dimethylaminophenyl)-cyclohexenone

被引：0

作者：

Lobo, Gricela M. ^{[1
]}

Charris, Jaime E. ^{[1
]}

机构：

[1] Univ Cent Venezuela, Fac Farm, Lab Sintesis Organ, Caracas 1051, Venezuela

来源：

MOLBANK | 2005年 / 06期

关键词：

D O I：

10.3390/M452

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

A mixture of 4-dimethylaminochalcone 1 (0.25 g, 1.00 mmol), methyl acetoacetate (0.17 g, 1.5 mmol) in methanol (5.00 mL) and sodium metoxide (0.25 mg) was stirred at room temperature for 24 hour to give a yellow precipitate. Then it was filtered and washed with water. Recrystalized of the crude substance from methanol afforded pure cyclohexenone 2 (2.27 g, 97.00 %). © 2005 MDPI. All rights reserved.

引用

页数：2

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