DETERMINATION OF CAULERPENYNE, A TOXIN FROM THE GREEN-ALGA CAULERPA-TAXIFOLIA (CAULERPACEAE)

被引：11
|
作者：
VALLS, R
ARTAUD, J
AMADE, P
VINCENTE, N
PIOVETTI, L
机构：
[1] INSERM,U303,F-06230 VILLEFRANCHE MER,FRANCE
[2] UNIV AIX MARSEILLE 3,CTR ETUD RESSOURCES ANIM MARINES,F-13397 MARSEILLE 13,FRANCE
[3] UNIV TOULON & VAR,RECH CHIM MARINE ORGANOMET LAB,F-83857 LA GARDE,FRANCE
来源：
JOURNAL OF CHROMATOGRAPHY A | 1994年 / 663卷 / 01期
关键词：
D O I：
10.1016/0021-9673(94)80502-4
中图分类号：
Q5 [生物化学];
学科分类号：
071010 ; 081704 ;
摘要：
A high-performance liquid chromatographic method is described for the determination of caulerpenyne, a neurotoxic sesquiterpenoid isolated from the green alga Caulerpa taxifolia. UV and refractometric detection were compared in order to determine the amounts of this toxin in the alga and the alimentary chain. UV detection at 252 nm was more sensitive and could be applied to the determination of very low concentrations of caulerpenyne (the detection limit per gram of dried seaweed was 27 mu g/g). The chromatographic conditions adopted were a 5-mu m silica column with isocratic binary elution with ethyl acetate-hexane (23:77, v/v) at a flow-rate of 1 ml/min.
引用
收藏
页码：114 / 118
页数：5
相关论文
共 50 条
  • [41] CHLOROPHYLL-PROTEIN COMPLEXES OF A MARINE GREEN-ALGA, CAULERPA-CACTOIDES
    ANDERSON, JM
    WALDRON, JC
    THORNE, SW
    PLANT SCIENCE LETTERS, 1980, 17 (02): : 149 - 157
  • [42] Raman Spectroscopic Insights into the Chemical Gradients within the Wound Plug of the Green Alga Caulerpa taxifolia
    Weissflog, Ina A.
    Grosser, Katharina
    Braeutigam, Maximilian
    Dietzek, Benjamin
    Pohnert, Georg
    Popp, Juergen
    CHEMBIOCHEM, 2013, 14 (06) : 727 - 732
  • [43] FREE AMINO-ACIDS IN THE MARINE GREEN-ALGA CAULERPA-SIMPLICIUSCULA
    SMITH, MM
    GAYLER, KR
    BOTANICA MARINA, 1979, 22 (06) : 361 - 365
  • [44] SELECTIVE ELIMINATION OF CHLOROPLASTIDIAL DNA FOR METAGENOMICS OF BACTERIA ASSOCIATED WITH THE GREEN ALGA CAULERPA TAXIFOLIA (BRYOPSIDOPHYCEAE)
    Aires, Tania
    Marba, Nuria
    Serrao, Ester A.
    Duarte, Carlos M.
    Arnaud-Haond, Sophie
    JOURNAL OF PHYCOLOGY, 2012, 48 (02) : 483 - 490
  • [45] Impacts of detritus from the invasive alga Caulerpa taxifolia on a soft sediment community
    Taylor, Skye L.
    Bishop, Melanie J.
    Kelaher, Brendan P.
    Glasby, Tim M.
    MARINE ECOLOGY PROGRESS SERIES, 2010, 420 : 73 - 81
  • [46] A new polyacetylenic fatty acid and other secondary metabolites from the Chinese green alga Caulerpa racemosa (Caulerpaceae) and their chemotaxonomic significance
    Mao, Shui-Chun
    Liu, Ding-Quan
    Yu, Xiao-Qing
    Lai, Xiao-Ping
    BIOCHEMICAL SYSTEMATICS AND ECOLOGY, 2011, 39 (4-6) : 253 - 257
  • [47] SESQUITERPENOID CAULERPENYNE LEVELS OF NEWLY IDENTIFIED CAULERPA TAXIFOLIA VAR. DISTICHOPHYLLA FROM THE ISKENDERUN BAY, TURKEY
    Cevik, Fatma
    Cavas, Levent
    Cevik, Cem
    Derici, Osman Baric
    Turkmen, Gizem
    Alyuruk, Hakan
    Gundogdu, Sedat
    FRESENIUS ENVIRONMENTAL BULLETIN, 2016, 25 (08): : 2867 - 2876
  • [48] ACTIN-BASED CHLOROPLAST REARRANGEMENTS IN THE CORTEX OF THE GIANT COENOCYTIC GREEN-ALGA CAULERPA
    MENZEL, D
    ELSNERMENZEL, C
    PROTOPLASMA, 1989, 150 (01) : 1 - 8
  • [49] Spread of the green alga Caulerpa taxifolia (Caulerpales, Chlorophyta) in the Mediterranean: Possible consequences of a major ecological event
    Boudouresque, CF
    Meinesz, A
    Ribera, MA
    Ballesteros, E
    SCIENTIA MARINA, 1995, 59 : 21 - 29
  • [50] Lack of epifaunal response to the application of salt for managing the noxious green alga Caulerpa taxifolia in a coastal lake
    O'Neill, K. M.
    Schreider, M. J.
    Glasby, T. M.
    Redden, A. R.
    HYDROBIOLOGIA, 2007, 580 (1) : 135 - 142
12345