A COMPARISON OF ULTRASONIC EXTRACTION AND SOXHLET EXTRACTION OF POLYCYCLIC AROMATIC-HYDROCARBONS FROM SEDIMENTS AND AIR PARTICULATE MATERIAL

被引：47
|
作者：
MARVIN, CH
ALLAN, L
MCCARRY, BE
BRYANT, DW
机构：
[1] MCMASTER UNIV,DEPT CHEM,HAMILTON L8S 4M1,ONTARIO,CANADA
[2] MCMASTER UNIV,DEPT BIOCHEM,HAMILTON L8S 4L8,ONTARIO,CANADA
来源：
INTERNATIONAL JOURNAL OF ENVIRONMENTAL ANALYTICAL CHEMISTRY | 1992年 / 49卷 / 04期
关键词：
ULTRASONIC EXTRACTION; POLYCYCLIC AROMATIC HYDROCARBONS;
D O I：
10.1080/03067319208027573
中图分类号：
O65 [分析化学];
学科分类号：
070302 ; 081704 ;
摘要：
The extraction of polycyclic aromatic hydrocarbons (PAH) from sediments and from an urban dust standard reference material (SRM 1649) was compared using two methods; ultrasonication and Soxhlet extraction. Sample weights ranging from 0.5 g to 5 g were extracted using ultrasonication. The yield of organic material from sediment samples using ultrasonication with two solvents was 2.53 +/- 0.10% while the Soxhlet method yielded 2.41 +/- 0.14% of the initial sample weight. Sequential ultrasonic extraction with two solvents was much more rapid (45 minutes) than Soxhlet extraction (two days) and resulted in equal extraction efficiency. The levels of PAH extracted by ultrasonication from the urban dust standard reference material varied by no more than 15% from the certified values.
引用
收藏
页码：221 / 230
页数：10
相关论文
共 50 条
  • [1] Comparison between Soxhlet, ultrasonic and microwave assisted extraction of polycyclic aromatic hydrocarbons from atmospheric particulate matter
    Piñeiro-Iglesias, M
    López-Mahía, P
    Vázquez-Blanco, E
    Muniategui-Lorenzo, S
    Prado-Rodríguez, D
    [J]. FRESENIUS ENVIRONMENTAL BULLETIN, 2000, 9 (1-2): : 17 - 22
  • [2] COMPARISON OF SUPERCRITICAL-FLUID EXTRACTION AND SOXHLET EXTRACTION FOR THE ANALYSIS OF NATIVE POLYCYCLIC AROMATIC-HYDROCARBONS IN SOILS
    REIMER, G
    SUAREZ, A
    [J]. JOURNAL OF CHROMATOGRAPHY A, 1995, 699 (1-2) : 253 - 263
  • [3] Comparison of pressurized fluid extraction, Soxhlet extraction and sonication for the determination of polycyclic aromatic hydrocarbons in urban air and diesel exhaust particulate matter
    Rynö, M
    Rantanen, L
    Papaioannou, E
    Konstandopoulos, AG
    Koskentalo, T
    Savela, K
    [J]. JOURNAL OF ENVIRONMENTAL MONITORING, 2006, 8 (04): : 488 - 493
  • [4] SUPERCRITICAL FLUID EXTRACTION OF NITRATED POLYCYCLIC AROMATIC-HYDROCARBONS AND POLYCYCLIC AROMATIC-HYDROCARBONS FROM DIESEL EXHAUST PARTICULATE MATTER
    PASCHKE, T
    HAWTHORNE, SB
    MILLER, DJ
    WENCLAWIAK, B
    [J]. JOURNAL OF CHROMATOGRAPHY, 1992, 609 (1-2): : 333 - 340
  • [5] Ultrasonic micellar extraction of polycyclic aromatic hydrocarbons from marine sediments
    Pino, V
    Ayala, JH
    Afonso, AM
    González, V
    [J]. TALANTA, 2001, 54 (01) : 15 - 23
  • [6] EXTRACTION OF POLYCYCLIC AROMATIC-HYDROCARBONS FROM SOILS
    MALISZEWSKAKORDYBACH, B
    [J]. CHEMIA ANALITYCZNA, 1991, 36 (04): : 719 - 725
  • [7] EXTRACTION OF POLYCYCLIC AROMATIC-HYDROCARBONS FROM HIGHLY CONTAMINATED SOILS - A COMPARISON BETWEEN SOXHLET, MICROWAVE AND SUPERCRITICAL-FLUID EXTRACTION TECHNIQUES
    DEAN, JR
    BARNABAS, IJ
    FOWLIS, IA
    [J]. ANALYTICAL PROCEEDINGS, 1995, 32 (08): : 305 - 308
  • [8] SUPERCRITICAL CARBON-DIOXIDE EXTRACTION OF POLYCYCLIC AROMATIC-HYDROCARBONS FROM SEDIMENTS
    LEE, HB
    PEART, TE
    HONGYOU, RL
    GERE, DR
    [J]. JOURNAL OF CHROMATOGRAPHY A, 1993, 653 (01) : 83 - 91
  • [9] COMPARISON OF SOXHLET AND SHAKE EXTRACTION OF POLYCYCLIC AROMATIC-HYDROCARBONS FROM COAL-TAR POLLUTED SOILS SAMPLED IN THE FIELD
    LINDHARDT, B
    HOLST, H
    CHRISTENSEN, TH
    [J]. INTERNATIONAL JOURNAL OF ENVIRONMENTAL ANALYTICAL CHEMISTRY, 1994, 57 (01) : 9 - 19
  • [10] EXTRACTION OF POLYCYCLIC AROMATIC-HYDROCARBONS FROM SPIKED SOIL
    COOVER, MP
    SIMS, RC
    DOUCETTE, W
    [J]. JOURNAL OF THE ASSOCIATION OF OFFICIAL ANALYTICAL CHEMISTS, 1987, 70 (06): : 1018 - 1020
12345