CRYSTAL-STRUCTURE OF LIGNOCAINE TETRACHLOROFERRATE(III) COMPLEX

被引：0

作者：

BABU, AM ^{[1
]}

SRIDHAR, MA ^{[1
]}

BELLAD, SB ^{[1
]}

INDIRA, A ^{[1
]}

ABDOH, MMM ^{[1
]}

PRASAD, JS ^{[1
]}

机构：

[1] AN NAJAH NATL UNIV,DEPT PHYS,W BANK,ISRAEL

来源：

ZEITSCHRIFT FUR KRISTALLOGRAPHIE | 1993年 / 203卷

关键词：

CRYSTAL STRUCTURE; LIGNOCAINE TETRACHLOROFERRATE(III);

D O I：

10.1524/zkri.1993.203.Part-2.161

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

The crystal structure of lignocaine tetrachloroferrate(III) complex, FeCl14H22N2OCl4, has been determined by X-ray diffraction using CuKalpha radiation. The compound crystallizes in triclinic space group P1BAR with unit cell parameters a = 8.7151(2) angstrom, b = 10.147(2) angstrom, c = 12.215(3) angstrom, alpha = 107.19(2)-degrees, beta = 106.29(2)-degrees, gamma = 92.69(2)-degrees with V = 980.5(4) angstrom3, Z = 2, D(m) = 1.441 Mg . m-3, D(c) = 1.463 Mg. M-3, mu = 22.75 mm-1. The structure was solved using 2728 reflections [I > 2.5sigma(I)] out of 3230 reflections by MULTAN. The final residuals are R(f) = 0.085 (R(w) = 0.106).

引用

页码：161 / 166

页数：6

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