INVESTIGATION OF THE COMPOSITION OF PINUS PEUCE NEEDLE OIL BY GC-MS AND GC-GC-MS

被引:30
|
作者
HENNIG, P [1 ]
STEINBORN, A [1 ]
ENGEWALD, W [1 ]
机构
[1] UNIV LEIPZIG,INST ANALYT CHEM,D-04103 LEIPZIG,GERMANY
关键词
GAS CHROMATOGRAPHY; ENANTIOSELECTIVITY; GC-MS; GC-GC-MS; PINUS PEUCE; MONOTERPENES;
D O I
10.1007/BF02269622
中图分类号
Q5 [生物化学];
学科分类号
071010 ; 081704 ;
摘要
Needles of the Macedonian Pine, Pinus peuce Griseb., a conifer growing in the Balkan mountains, were extracted by a Likens-Nickerson simultaneous distillation-solvent extraction device. The components of this essential oil were identified by the retention times obtained on two columns differing in polarity and by GC-MS. Because of the complex nature of such plant extracts, a multidimensional GC method for enantiomer analysis, a multidimensional GC method for enantiomer analysis, using a non-chiral pre-column and a chiral main column has been developed. The enantiomeric ratios of five monoterpene hydrocarbons were estimated by GC-GC and GC-GC-MS.
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页码:689 / 693
页数:5
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