3,5-Bis(4-dodecylthiophen-2-yl)-4H-1,2,6-thiadiazin-4-one

被引：0
|
作者：
Ioannidou, Heraklidia A. [1 ]
Koutentis, Panayiotis A. [1 ]
机构：
[1] Univ Cyprus, Dept Chem, POB 20537, CY-1678 Nicosia, Cyprus
来源：
MOLBANK | 2012年 / 04期
关键词：
1,2,6-thiadiazines; thiophenes; heterocycles; oligomers;
D O I：
10.3390/M784
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
3,5-Dichloro-4H-1,2,6-thiadiazin-4-one 1 reacts with (4-dodecylthiophen-2yl) trimethylstannane 4 (2.2 equiv.) and Pd(Ph3P)(2)Cl-2 (5 mol%) in acetonitrile at ca. 82 degrees C to give 3,5-bis(4-dodecylthiophen-2-yl)-4H-1,2,6-thiadiazin-4-one 5 in 93% yield.
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页数：3
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