3,5-Bis(4-dodecylthiophen-2-yl)-4H-1,2,6-thiadiazin-4-one

被引：0
|
作者：
Ioannidou, Heraklidia A. [1 ]
Koutentis, Panayiotis A. [1 ]
机构：
[1] Univ Cyprus, Dept Chem, POB 20537, CY-1678 Nicosia, Cyprus
来源：
MOLBANK | 2012年 / 04期
关键词：
1,2,6-thiadiazines; thiophenes; heterocycles; oligomers;
D O I：
10.3390/M784
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
3,5-Dichloro-4H-1,2,6-thiadiazin-4-one 1 reacts with (4-dodecylthiophen-2yl) trimethylstannane 4 (2.2 equiv.) and Pd(Ph3P)(2)Cl-2 (5 mol%) in acetonitrile at ca. 82 degrees C to give 3,5-bis(4-dodecylthiophen-2-yl)-4H-1,2,6-thiadiazin-4-one 5 in 93% yield.
引用
收藏
页数：3
相关论文
共 50 条
  • [1] 3-Chloro-5-(4-dodecylthiophen-2-yl)-4H-1,2,6-thiadiazin-4-one
    Ioannidou, Heraklidia A.
    Koutentis, Panayiotis A.
    MOLBANK, 2012, (04)
  • [2] 3,5-Bis[5-(thiazol-2-yl)thien-2-yl]-4H-1,2,6-thiadiazin-4-one
    Kalogirou, Andreas S.
    Koutentis, Panayiotis A.
    MOLBANK, 2019, (01)
  • [3] 3,5-DICHLORO-4H-1,2,6-THIADIAZIN-4-ONE
    HARKEMA, S
    ACTA CRYSTALLOGRAPHICA SECTION B-STRUCTURAL SCIENCE, 1978, 34 (SEP): : 2927 - 2928
  • [4] 3-Chloro-5-(3-n-hexylthien-2-yl)-4H-1,2,6-thiadiazin-4-one
    Kalogirou, Andreas S.
    Koutentis, Panayiotis A.
    MOLBANK, 2019, (01)
  • [5] SYNTHESIS AND REACTIONS OF 3,5-DICHLORO-4H-1,2,6-THIADIAZIN-4-ONE
    GEEVERS, J
    TROMPEN, WP
    RECUEIL DES TRAVAUX CHIMIQUES DES PAYS-BAS-JOURNAL OF THE ROYAL NETHERLANDS CHEMICAL SOCIETY, 1974, 93 (9-10): : 270 - 272
  • [6] 5,5′-Thiobis(3-methoxy-4H-1,2,6-thiadiazin-4-one)
    Kalogirou, Andreas S.
    Koutentis, Panayiotis A.
    MOLBANK, 2019, (02)
  • [7] Palladium Catalyzed C-C Coupling Reactions of 3,5-Dichloro-4H-1,2,6-thiadiazin-4-one
    Ioannidou, Heraklidia A.
    Kizas, Christos
    Koutentis, Panayiotis A.
    ORGANIC LETTERS, 2011, 13 (13) : 3466 - 3469
  • [8] Substitution at C-4 in 3,5-disubstituted 4H-1,2,6-thiadiazin-4-ones
    Ioannidou, Heraklidia A.
    Koutentis, Panayiotis A.
    TETRAHEDRON, 2012, 68 (12) : 2590 - 2597
  • [9] Synthesis of 2-(4H-1,2,6-thiadiazin-4-ylidene)malononitriles
    Kalogirou, Andreas S.
    Koutentis, Panayiotis A.
    TETRAHEDRON, 2014, 70 (44) : 8334 - 8342
  • [10] 3,5-Bis(4-methoxyphenyl)-4H-1,2,4-triazol-4-amine
    Yang, Hui
    Huang, Zhan-Dong
    Yang, Guang
    Ng, Seik Weng
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : O2236 - U1662
12345