Crystal structure of N-(quinolin-6-yl)hydroxylamine

被引：1

作者：

Rajapakse, Anuruddha ^{[1
]}

Hillebrand, Roman ^{[1
]}

Lewis, Sarah M. ^{[1
]}

Parsons, Zachary D. ^{[1
]}

Barnes, Charles L. ^{[1
]}

Gates, Kent S. ^{[1
]}

机构：

[1] Univ Missouri, 125 Chem Bldg, Columbia, MO 65211 USA

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2014年 / 70卷

基金：

美国国家卫生研究院;

关键词：

crystal structure; N-arylhydroxylamine; hydroxylamine; N-(quinolin-6yl)hydroxylamine; quinoline;

D O I：

10.1107/S160053681402193X

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

The title compound, C9H8N2O, crystallized with four independent molecules in the asymmetric unit. The four molecules are linked via one O-H...N and two N-H...N hydrogen bonds, forming a tetramer-like unit. In the crystal, molecules are further linked by O-H...N and N-H...O hydrogen bonds forming layers parallel to (001). These layers are linked via C-H...O hydrogen bonds and a number of weak C-H...pi interactions, forming a three-dimensional structure. The crystal was refined as a non-merohedral twin with a minor twin component of 0.319.

引用

页码：322 / +

页数：11

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