APPLICATION OF 2 RAPID TECHNIQUES OF COLUMN CHROMATOGRAPHY TO SEPARATE THE PUNGENT PRINCIPLES OF GINGER, ZINGIBER-OFFICINALE ROSCOE

被引：9

作者：

ZARATE, R

SUKRASNO

YEOMAN, MM

机构：

[1] Institute of Cell and Molecular Biology, University of Edinburgh, Edinburgh, EH9 3JH Scotland, Daniel Rutherford Building, Mayfield Rd.

来源：

JOURNAL OF CHROMATOGRAPHY | 1992年 / 609卷 / 1-2期

关键词：

D O I：

10.1016/0021-9673(92)80189-2

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

Two rapid techniques of column chromatography, flash chromatography and vacuum chromatography, together with solvent systems differing in polarity, have been used to separate the pungent principles (gingerols and shogaols) of an extract of ginger powder. Gingerols consist of a homologous series of aldols each containing a phenolic group which together with shogaols, showing similar structure, give the pungency of ginger. Thin-layer chromatographic analysis of the fractions collected from both chromatographic techniques showed that the main gingerol homologues are separated satisfactorily from the other compounds only using vacuum chromatography. These compounds were eluted with hexane-diethyl ether (30:70) and (20:80) respectively. The results obtained with flash chromatography, on the other hand, were not satisfactory.

引用

页码：407 / 413

页数：7

共 50 条

[41] Rapid detection of adulteration in powder of ginger (Zingiber officinale Roscoe) by FT-NIR spectroscopy combined with chemometrics
Yu, Dai-xin
Guo, Sheng
Zhang, Xia
Yan, Hui
Zhang, Zhen-yu
Chen, Xin
Chen, Jiang-yan
Jin, Shan-jie
Yang, Jian
Duan, Jin-ao
FOOD CHEMISTRY-X, 2022, 15
[42] IDENTIFICATION OF THE CHARACTERISTIC ODORANTS IN FRESH RHIZOMES OF GINGER (ZINGIBER-OFFICINALE ROSCOE) USING AROMA EXTRACT DILUTION ANALYSIS AND MODIFIED MULTIDIMENSIONAL GAS-CHROMATOGRAPHY MASS-SPECTROSCOPY
NISHIMURA, O
JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 1995, 43 (11) : 2941 - 2945
[43] GAS-CHROMATOGRAPHIC ANALYSIS OF THERMAL-DEGRADATION PRODUCTS OF GINGEROL COMPOUNDS IN STEAM-DISTILLED OIL FROM GINGER (ZINGIBER-OFFICINALE ROSCOE)
CHEN, CC
HO, CT
JOURNAL OF CHROMATOGRAPHY, 1987, 387 : 499 - 504
[44] Comparison of the histology of (I) fresh, (II) solar dried and (III) solar dried steam distilled ginger (Zingiber officinale Roscoe) rhizome tissue prior to the extraction of its pungent principles
Balladin, DA
Headley, O
Chang-yen, I
Duncan, EJ
McGaw, DR
RENEWABLE ENERGY, 1999, 17 (02) : 207 - 211
[45] Enhanced intestinal uptake of iron, zinc and calcium in rats fed pungent spice principles - Piperine, capsaicin and ginger (Zingiber officinale)
Prakash, Usha N. S.
Srinivasan, Krishnapura
JOURNAL OF TRACE ELEMENTS IN MEDICINE AND BIOLOGY, 2013, 27 (03) : 184 - 190
[46] Antioxidant and inhibitory effect of red ginger (Zingiber officinale var. Rubra) and white ginger (Zingiber officinale Roscoe) on Fe2+ induced lipid peroxidation in rat brain in vitro
Oboh, Ganiyu
Akinyemi, Ayodele J.
Ademiluyi, Adedayo O.
EXPERIMENTAL AND TOXICOLOGIC PATHOLOGY, 2012, 64 (1-2) : 31 - 36
[47] Preparative separation and purification of gingerols from ginger (Zingiber officinale Roscoe) by high-speed counter-current chromatography
Zhan, Kunyou
Xu, Kun
Yin, Hongzong
FOOD CHEMISTRY, 2011, 126 (04) : 1959 - 1963
[48] Effect of CO2 Enrichment on Synthesis of Some Primary and Secondary Metabolites in Ginger (Zingiber officinale Roscoe)
Ghasemzadeh, Ali
Jaafar, Hawa Z. E.
INTERNATIONAL JOURNAL OF MOLECULAR SCIENCES, 2011, 12 (02) : 1101 - 1114
[49] Comparison of the Key Aroma Compounds in Fresh, Raw Ginger (Zingiber officinale Roscoe) from China and Roasted Ginger by Application of Aroma Extract Dilution Analysis
Schaller, Tanja
Schieberle, Peter
JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 2020, 68 (51) : 15292 - 15300
[50] Identification and Concentration of Some Flavonoid Components in Malaysian Young Ginger (Zingiber officinale Roscoe) Varieties by a High Performance Liquid Chromatography Method
Ghasemzadeh, Ali
Jaafar, Hawa Z. E.
Rahmat, Asmah
MOLECULES, 2010, 15 (09): : 6231 - 6243

← 1 2 3 4 5 →