N-(3-Chloro-1,4-dioxo-1,4-dihydronaphthalen-2-yl)-N-propionylpropionamide

被引：0
|
作者：
Idris, Nabil [1 ]
Butcher, Ray J. [1 ]
Bakare, Oladapo [1 ]
机构：
[1] Howard Univ, Dept Chem, 525 Coll St NW, Washington, DC 20059 USA
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2014年 / 70卷
基金：
美国国家卫生研究院;
关键词：
data-to-parameter ratio = 14.5; mean σ(C-C) = 0.003 Å; R factor = 0.042; single-crystal X-ray study; T = 123 K; wR factor = 0.115;
D O I：
10.1107/S1600536813034302
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
In the title molecule, C16H14ClNO4, the four essentially planar atoms of the imide group [r.m.s. deviation = 0.0286 (11) angstrom] form a dihedral angle of 77.36 (13)degrees with the naphthoquinone group [maximun deviation = 0.111 (2) angstrom for the carbonyl O atom in the naphthalene 1-position] and the two imide carbonyl groups are oriented anti with respect to each other. In the crystal, molecules are connected by weak C-H center dot center dot center dot O hydrogen bonds, as well as pi-pi stacking interactions [centroid-centroid distance = 3.888 (3) angstrom], forming a threedimensional network.
引用
收藏
页码：0102 / +
页数：8
相关论文
共 50 条
  • [31] Modulation of dual fluorescence modes and emissions of 2-(1,4-dioxo-1,4-dihydro-naphthalen-2-yl-amino)benzoic acid
    Singh, Munendra Pal
    Baruah, Jubaraj B.
    JOURNAL OF MOLECULAR STRUCTURE, 2017, 1149 : 315 - 322
  • [32] Syntesis of 2-and 3-chloro-1,4-dihydroxythioxanthen-9-ones
    Loskutov, V. A.
    Mamatyuk, V. I.
    Beregovaya, I. V.
    RUSSIAN JOURNAL OF ORGANIC CHEMISTRY, 2010, 46 (02) : 241 - 245
  • [33] Aqua(4,4′-bipyridine-κN)bis(1,4-dioxo-1,4-dihydronaphthalen-2-olato-κ2O1,O2)zinc 4,4′-bipyridine monosolvate dihydrate
    Silva, Marcos M. P.
    Carvalho, Lucas J.
    Lanznaster, Mauricio
    Resende, Jackson A. L. C.
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : M1489 - +
  • [34] Syntesis of 2- and 3-chloro-1,4-dihydroxythioxanthen-9-ones
    V. A. Loskutov
    V. I. Mamatyuk
    I. V. Beregovaya
    Russian Journal of Organic Chemistry, 2010, 46 : 241 - 245
  • [35] SYNTHESIS AND BIOLOGICAL-ACTIVITY OF SOME NEW N-(2H-1,4-BENZOXAZIN-3-YL AND BENZOTHIAZIN-3-YL)-N'-ARYLUREAS
    SHRIDHAR, DR
    SASTRY, CVR
    BANSAL, OP
    RAO, PP
    INDIAN JOURNAL OF CHEMISTRY SECTION B-ORGANIC CHEMISTRY INCLUDING MEDICINAL CHEMISTRY, 1986, 25 (08): : 874 - 876
  • [36] Synthesis of new (3,4-dihydro-3-oxo-2H-1,4-benzoxazin-2-yl)-N-( 4-aryl-3-chloro-2-oxo-azetidin-1-yl) acetamides
    Jayamma, Y
    Patnaik, S
    Kalyane, N
    Reddy, VM
    INDIAN JOURNAL OF HETEROCYCLIC CHEMISTRY, 2003, 12 (04) : 351 - 354
  • [37] N-[(2-Chloro-6-methylquinolin-3-yl) methyl]aniline
    Kumar, Suresh
    Bawa, Sandhya
    Drabu, Sushma
    MOLBANK, 2009, (03)
  • [38] Preparation of N-(4-methylpentane-2-yl) N′-[2-(2-phenylpropane-2-yl)]-benzene-1,4-diamine
    Sigmundová, I
    Uhlár, J
    Toma, S
    SYNTHETIC COMMUNICATIONS, 2004, 34 (20) : 3667 - 3672
  • [39] N-[3-(4-Fluorobenzyl)-2,4-dioxo-1,3-diazaspiro[4.5]dec-8-yl]-2-methylbenzenesulfonamide
    Jeyaseelan, S.
    Vinduvahini, M.
    Madaiah, M.
    Bhattacharya, Suman
    Revanasiddappa, H. D.
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2012, 68
  • [40] I2/TBHP mediated domino synthesis of 2(2,4-dioxo-1,4-dihydroquinazolin-3(2H)-yl)-N-aryl/alkyl benzamides and evaluation of their anticancer and docking studies
    Soda, Anil Kumar
    Krishna, Phani C. S.
    Chilaka, Sai Krishna
    Krishna, Vamshi E.
    Misra, Sunil
    Madabhushi, Sridhar
    RSC ADVANCES, 2022, 12 (26) : 16589 - 16598
12345