PRELIMINARY-STUDY ON THE USE OF PALLADIUM AS A CHEMICAL MODIFIER FOR THE DETERMINATION OF SILICON BY ELECTROTHERMAL ATOMIC-ABSORPTION SPECTROMETRY

被引：19
|
作者：
ZHUANG, ZX [1 ]
YANG, PY [1 ]
WANG, XR [1 ]
DENG, ZW [1 ]
HUANG, BL [1 ]
机构：
[1] XIAMEN UNIV,DEPT CHEM,XIAMEN 361005,PEOPLES R CHINA
来源：
JOURNAL OF ANALYTICAL ATOMIC SPECTROMETRY | 1993年 / 8卷 / 08期
关键词：
ELECTROTHERMAL ATOMIC ABSORPTION SPECTROMETRY; PALLADIUM MODIFIER; SILICON DETERMINATION; LOW ALLOY STEEL SAMPLES;
D O I：
10.1039/ja9930801109
中图分类号：
O65 [分析化学];
学科分类号：
070302 ; 081704 ;
摘要：
This paper describes the use of palladium salt as chemical modifier for the determination of silicon by electrothermal atomic absorption spectrometry. It is found that the optimal atomization temperature of silicon appeared to be flat above 2500-degrees-C and that the sensitivity was significantly improved in the presence of palladium. The method was validated by the analysis of National Bureau of Standards (now National Institute for Standards and Technology) Standard Reference Materials 361, 362 and 363 Low Alloy Steels.
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页码：1109 / 1111
页数：3
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