SYNTHESIS OF A CELL-WALL COMPONENT OF HAEMOPHILUS (ACTINOBACILLUS) PLEUROPNEUMONIAE SEROTYPE-5

被引：15
|
作者：
VANDERKLEIN, PAM
FILEMON, W
BOONS, GJPH
VEENEMAN, GH
VANDERMAREL, GA
VANBOOM, JH
机构：
[1] Gorlaeus Laboratories, 2300 RA Leiden
来源：
TETRAHEDRON | 1992年 / 48卷 / 22期
关键词：
D O I：
10.1016/S0040-4020(01)81239-4
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
The disaccharide alpha-D-GlcNAcp-(1-5)-beta-KDO-2-OCH2CH2CH2NH2 containing a spacer beta-linked to KDO is prepared via iodonium ion-assisted glycosylation of a suitable KDO acceptor with ethyl 2-azido-2-deoxy-3,4-di-O-benzyl-1-thio-alpha/beta-D-glucopyranoside. The key KDO building unit is synthesized in 7 steps starting with 2,3:5,6-di-O-isopropylidene-D-mannitol.
引用
收藏
页码：4649 / 4658
页数：10
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