QUANTITATIVE FOURIER-TRANSFORM INFRARED ATTENUATED TOTAL REFLECTANCE ANALYSIS OF KETOPROFEN IN SOME PHARMACEUTICAL FORMULATIONS

被引：16

作者：

VANOVERBEKE, A

BAEYENS, W

VANDENBOSSCHE, W

机构：

[1] Laboratory of Drug Analysis, Department of Pharmaceutical Analysis, Faculty of Pharmaceutical Sciences, B-9000 Ghent

来源：

VIBRATIONAL SPECTROSCOPY | 1995年 / 9卷 / 02期

关键词：

ATTENUATED TOTAL REFLECTANCE; INFRARED SPECTROMETRY; KETOPROFEN; PHARMACEUTICALS;

D O I：

10.1016/0924-2031(94)00090-4

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

An overhead attenuated total reflectance system was used to quantify ketoprofen in some pharmaceutical formulations (capsules and injection ampoules). No extensive sample pretreatment was needed. The ampoules were analysed as such and a simultaneous quantification of ketoprofen and arginine base was performed. A partial least-squares package (PLS1) was applied to the calibration and prediction for a limited number of standard solutions.

引用

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页码：121 / 130

页数：10

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