FACILE INTRODUCTION OF N-15 INTO CHALCOGEN NITROGEN SYSTEMS USING N-15-LABELED AMMONIA

被引：14

作者：

GINN, VC ^{[1
]}

KELLY, PF ^{[1
]}

WOOLLINS, JD ^{[1
]}

机构：

[1] UNIV LONDON IMPERIAL COLL SCI TECHNOL & MED,DEPT CHEM,S KENSINGTON,LONDON SW7 2AY,ENGLAND

来源：

JOURNAL OF THE CHEMICAL SOCIETY-DALTON TRANSACTIONS | 1992年 / 13期

关键词：

D O I：

10.1039/dt9920002129

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

Reaction of N-15-labelled ammonia with a toluene solution of (EtO)2SeO under reduced pressure gives (Se4N4)-N-15; in the presence of [PtCl2(PMe2Ph)2] (with CH2Cl2 as solvent) the same reagents yield [Pt(Se2N2)-N-15 (PMe2Ph)2] whilst (NH3)-N-15, [PtCl2(PMe2Ph)2] and SOCl2 react to form [Pt(NSO)2)-N-15-(PMe2Ph)2].

引用

页码：2129 / 2130

页数：2

共 50 条

[1] A convenient synthesis of N-15-labeled diethylenetriamine [(N-15)Dien] and ethylenediamine [(N-15)En]
Zang, E
Sadler, PJ
[J]. SYNTHESIS-STUTTGART, 1997, (04): : 410 - &
[2] RELATIVE CONCENTRATIONS OF N-15 IN URINARY AMMONIA N AND UREA N AFTER FEEDING N-15-LABELED COMPOUNDS
WU, H
[J]. JOURNAL OF GENERAL PHYSIOLOGY, 1951, 34 (04): : 403 - 409
[3] N-15 NUCLEAR MAGNETIC-RESONANCE SPECTROSCOPY OF N-15-LABELED NUCLEOTIDES
BUCHNER, P
MAURER, W
RUTERJANS, H
[J]. JOURNAL OF MAGNETIC RESONANCE, 1978, 29 (01) : 45 - 63
[4] NITROGEN-15-LABELED OLIGODEOXYNUCLEOTIDES - CHARACTERIZATION BY N-15 NMR OF D[CGTACG] CONTAINING N-15(6)-LABELED OR N-15(1)-LABELED DEOXYADENOSINE
GAO, X
JONES, RA
[J]. JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1987, 109 (10) : 3169 - 3171
[5] UPTAKE AND REDISTRIBUTION OF N-15 WITHIN AN ESTABLISHED ASPARAGUS CROP AFTER APPLICATION OF N-15-LABELED NITROGEN-FERTILIZER
LEDGARD, SF
DOUGLAS, JA
SPROSEN, MS
FOLLETT, JM
[J]. ANNALS OF BOTANY, 1994, 73 (02) : 169 - 173
[6] N-15 MAGNETIC-RESONANCE STUDIES OF BINDING OF N-15-LABELED CYANIDE TO VARIOUS HEMOPROTEINS
MORISHIMA, I
INUBUSHI, T
NEYA, S
OGAWA, S
YONEZAWA, T
[J]. BIOCHEMICAL AND BIOPHYSICAL RESEARCH COMMUNICATIONS, 1977, 78 (02) : 739 - 746
[7] DETECTION OF N-15-LABELED AMMONIUM - INVIVO N-15 NMR VERSUS MASS-SPECTROMETRY
FOX, GG
RATCLIFFE, RG
ROBINSON, SA
SLADE, AP
STEWART, GR
[J]. JOURNAL OF MAGNETIC RESONANCE, 1992, 96 (01): : 146 - 153
[8] N-15 NMR-STUDIES OF BINDING OF N-15-LABELED CYANIDE TO VARIOUS HEMOGLOBINS IN INTACT ERYTHROCYTE
MORISHIMA, I
INUBUSHI, T
[J]. BIOCHEMICAL AND BIOPHYSICAL RESEARCH COMMUNICATIONS, 1978, 80 (01) : 199 - 205
[9] RATE OF EXCRETION OF N-15 AFTER FEEDING N-15-LABELED L-ASPARTIC ACID IN MAN
WU, H
SNYDERMAN, SE
[J]. JOURNAL OF GENERAL PHYSIOLOGY, 1951, 34 (03): : 339 - 345
[10] STUDIES ON THE NITROGEN METABOLISM OF TOMATO USING N-15-LABELED AMMONIUM SULFATE
MACVICAR, R
BURRIS, RH
[J]. FEDERATION PROCEEDINGS, 1948, 7 (01) : 170 - 171

← 1 2 3 4 5 →