THIENYLPYRIDINES AS A NEW FLUORESCENT REAGENT .2. DETERMINATION OF CARBOXYLIC-ACID WITH 5-(4-PYRIDYL)-2-THIOPHENEMETHANOL USING HPLC

被引：5
|
作者：
NAKAJIMA, R
SHIMADA, K
FUJII, Y
YAMAMOTO, A
HARA, T
机构：
[1] Department of Chemical Engineering, Faculty of Engineering, Doshisha University, Kamigyo, Kyoto
来源：
BULLETIN OF THE CHEMICAL SOCIETY OF JAPAN | 1991年 / 64卷 / 10期
关键词：
D O I：
10.1246/bcsj.64.3173
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
The title compound has been prepared and used as a new derivatization reagent. The reagent reacts with the carboxylic acids in chloroform in the presence of 1-isopropyl-3-(3-dimethylaminopropyl)carbodiimide to produce the corresponding fluorescent esters, which can be separated on an octadecyl-silica column. Each 5 fmol of hexadecanoic or octadecanoic acids and about 50 fmol of benzoic and p-anisic acids (1-mu-l injection) (S/N = 2) were detected.
引用
收藏
页码：3173 / 3175
页数：3
相关论文
共 50 条
  • [1] THIENYLPYRIDINES AS A NEW FLUORESCENT REAGENT .1. DETERMINATION OF PRIMARY ALKYLAMINES WITH 5-(4-PYRIDYL)-2-THIOPHENECARBALDEHYDE USING HPLC
    NAKAJIMA, R
    YAMAMOTO, A
    HARA, T
    BULLETIN OF THE CHEMICAL SOCIETY OF JAPAN, 1990, 63 (07) : 1968 - 1972
  • [2] SYNTHESIS AND SPECTRAL PROPERTIES OF 5,5'-DI(4-PYRIDYL)-2,2'-BITHIENYL AS A NEW FLUORESCENT COMPOUND
    NAKAJIMA, R
    IIDA, H
    HARA, T
    BULLETIN OF THE CHEMICAL SOCIETY OF JAPAN, 1990, 63 (02) : 636 - 637
  • [3] Synthesis of a new reagent 3-(4′-fluorophenyl)-5-(2′-carboxylphenylazo) rhodanine and the fluorescent determination of bismuth(III)
    Yu, JH
    Ou, QY
    Li, T
    Wang, LG
    CHINESE JOURNAL OF ANALYTICAL CHEMISTRY, 2004, 32 (05) : 644 - 646
  • [4] Selective Recognition of Zn2+ Ion Using 2,4-Bis(2-pyridyl)-5-(4-pyridyl) imidazole: Spectra and Molecular Structure
    Behera, Nibedita
    Manivannan, Vadivelu
    CHEMISTRYSELECT, 2016, 1 (13): : 4016 - 4023
  • [5] Synthesis, Crystal Structure, Fluorescent Property and DFT Calculations of a New Zn(Ⅱ) Complex Based on 3-(2-Pyridyl)-5-(4-pyridyl)-1H-1,2,4-triazole
    靳晓东
    李冰
    高慧
    张霞
    刘万毅
    结构化学, 2016, 35 (07) : 1129 - 1136
  • [6] pH Dependent Synthesis of NdIII Coordination Compounds Based on Bifunctional 5-(4-Pyridyl)tetrazole-2-acetic Acid
    Cao, Meng Jie
    Li, Yue Kang
    Sun, Peng Peng
    Zhang, Chen Yi
    Wang, Jue
    Li, Qiao Yun
    Yang, Gao Wen
    ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE, 2016, 642 (21): : 1218 - 1221
  • [7] HPLC RESOLUTION OF HYDROXYL CARBOXYLIC-ACID ENANTIOMERS USING 2-QUINOXALOYL CHLORIDE AS A NEW PRECOLUMN DERIVATIZING AGENT
    BRIGHTWELL, M
    PAWLOWSKA, M
    ZUKOWSKI, J
    JOURNAL OF LIQUID CHROMATOGRAPHY, 1995, 18 (14): : 2765 - 2781
  • [8] 4-TRIFLUOROMETHYLIMIDAZOLES AND 5-(4-PYRIDYL)-1,2,4-TRIAZOLES, NEW CLASSES OF XANTHINE-OXIDASE INHIBITORS
    BALDWIN, JJ
    KASINGER, PA
    NOVELLO, FC
    SPRAGUE, JM
    DUGGAN, DE
    JOURNAL OF MEDICINAL CHEMISTRY, 1975, 18 (09) : 895 - 900
  • [9] Synthesis, Crystal Structure, Fluorescent Property and DFT Calculations of a New Zn(II) Complex Based on 3-(2-Pyridyl)-5-(4-pyridyl)-1H-1,2,4-triazole
    Jin Xiao-Dong
    Li Bing
    Gao Hui
    Zhang Xia
    Liu Wan-Yi
    CHINESE JOURNAL OF STRUCTURAL CHEMISTRY, 2016, 35 (07) : 1129 - 1136
  • [10] 4-(5,6-dimethoxy-2-phthalimidinyl)phenyl hydrazide as a fluorescent labeling reagent for determination of aldehydes in HPLC
    Inoue, H
    Yamazaki, J
    Sugino, E
    Fujioka, H
    Kohashi, K
    Date, Y
    Ishii, Y
    Tsuruta, Y
    ANALYTICAL SCIENCES, 1997, 13 (04) : 669 - 671
12345