4-Hydroxymethyl-10-methoxy-17,22-dioxapentacyclo[21.2.2.2(13,16).1(3,7).0(11,30)]triaconta-1(25),3,5,7(30),8,10,13,15,23,26,28-undecaene-2,12-dione acetone monosolvate

被引：0

作者：

Hijikata, Daichi ^{[1
]}

Sasagawa, Kosuke ^{[1
]}

Yoshiwaka, Sayaka ^{[1
]}

Okamoto, Akiko ^{[1
]}

Yonezawa, Noriyuki ^{[1
]}

机构：

[1] Tokyo Univ Agr & Technol, Dept Organ & Polymer Mat Chem, Koganei, Tokyo 1848588, Japan

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2012年 / 68卷

关键词：

D O I：

10.1107/S1600536812033521

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

In the title compound, C30H26O6 center dot C3H6O, the syn-oriented benzoyl groups are nearly parallel to each other; the dihedral angle between their benzene rings is 15.9 (1)degrees. They form dihedral angles of 72.5 (1) and 84.3 (1)degrees with the naphthalene system. In the crystal, molecules are linked into a threedimensional architecture by C-H center dot center dot center dot O and C-H center dot center dot center dot pi interactions.

引用

页码：02598 / +

页数：13

共 19 条

[1] anti-2,2,3,3,6,6,7,7,10,10,11,11,14,14,15,15-Hexadecamethy1-2,3,6,7,10,11,- 14,15-octasilapentacyclo[1 0.4.2.2(4'9).0(5'8).0(13'16)]icosa-1 (1 7),4,8,12(18),13(1 6),19-hexaene
Toma, Yuki
Otsuka, Kyohei
Kyushin, Soichiro
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2013, 69 : O341 - +
[2] 11,28-BIS(CHLOROACETYL)-6,7,9,10,12,13,15,16,23,24,26,27,29,30,32,33-HEXADECAHYDRO-DIBENZO[B,Q][1,4,7,10,16,19,22,25,13,28]OCTAOXADIAZACYCLOTRIACONTINE
ANELLI, PL
STODDART, JF
SLAWIN, AMZ
WILLIAMS, DJ
ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1990, 46 : 1464 - 1467
[3] CRYSTAL-STRUCTURE OF 2,8,14,20-TETRAMETHYLPENTACYCLO-[19.3.1.1(3,7).1(9,13)1(15,19)]OCTACOSA-1-(25),3,5,7(28),9,11,13(27),15,17,19(26),21,23-DODECAENE-4,6,10,12,16,18,22,24-OCTAETHYL ETHER, C48H64O8
ZAHN, G
MULLER, K
MANN, G
ZEITSCHRIFT FUR KRISTALLOGRAPHIE, 1994, 209 (05): : 473 - 474
[4] CRYSTAL-STRUCTURE OF 2,8,14,20-TETRAMETHYLPENTACYCLO-[19.3.1.1(3,7).1(9,13).1(15,19)]OCTACOSA-1-(25),3,5,7(28),9,11,13(27),15,17,19(26),21,23-DODECAENE-4,6,10,12,16,18,22,24-OCTOL, C32H32O8
ZAHN, G
SIELER, J
MULLER, K
HENNIG, L
MANN, G
ZEITSCHRIFT FUR KRISTALLOGRAPHIE, 1994, 209 (05): : 468 - 469
[5] (1 ' S, 12 ' R, 13 ' S, 17 ' S)-15 ',15 '-Dimethyl-1,2-dihydro-11 ',14 ',16 ',18 '-tetraoxa-7 '-azaspiro[indole-3,8 '-pentacyclo-[10.6.0.0(2,9).0(3,7).0(13,17)]octadecane]-2,10 '-dione
Sabari, V.
Ponnusamy, R.
Prasanna, R.
Raghunathan, R.
Aravindhan, S.
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2013, 69 : O466 - +
[6] 3,10,14,21-Tetrakis(4-methoxyphenyl)-pentacyclo[11.8.0.0(2,11).0(4,9).0(15,20)]-henicosa-1(21),2,4(9),5,7,10,13,15(20),-16,18-decaen-12-one chloroform monosolvate
Gopinath, S.
Narayanan, P.
Sethusankar, K.
Nandakumar, Meganathan
Mohanakrishnan, Arasambattu K.
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2014, 70 : O873 - +
[7] Synthesis, characterization and antimicrobial activities of homo- and bimetallic trinuclear complexes of a 30-membered macrocyclic ligand [30] 1,4,5,9,10,13, 16,19,20,24,25,28-dodecaaza-2,3,11,12,17,18,26,27-octaphenyl-6,8,21,23-tetramethylcyclotriaconta-1,3,5,8,10,12,16,18,20,23,25,27-dodecaene (L)
Tripathy, S. K.
Panda, A.
Das, P. K.
Behera, N. K.
Panda, A. K.
JOURNAL OF THE INDIAN CHEMICAL SOCIETY, 2014, 91 (07) : 1237 - 1245
[8] 1,9-diazaoctacyclo[22.6.1.13,7.19,16.218,31.010,15.221,16.024,29]tetratriaconta-3,5,7(30),10(15),11,13,16(31),17,19,21,23(36),24(29), 25,27,32,34-hexadecaene
Kumar, G. Senthil
Chinnakali, K.
Sekar, K.
Rajakumar, P.
Fun, Hoong-Kun
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2006, 62 : O3455 - O3456
[9] Final report on the safety assessment of Ceteareth-2,-3,-4,-5,-6,-7,-8,-9,-10,-11,-12,-13,-14,-15,-16,-17,-18,-20,-22,-23,-24,-25,-27,-28,-29,-30,-33,-34,-40,-50,-55,-60,-80, and-100
Madhaven, BM
INTERNATIONAL JOURNAL OF TOXICOLOGY, 1999, 18 : 41 - 49
[10] 17-(5-Ethyl-6-methylheptan-2-yl)-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthrene-3,7-diol from Chisocheton tomentosus (Meliaceae)
Najmuldeen, Ibrahim A.
Hadi, Abdul Hamid Abdul
Awang, Khalijah
Mohamad, Khalit
Ng, Seik Weng
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2008, 64 : O2163 - U2375

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