DETERMINATION OF NITROBENZENES IN RIVER WATER, SEDIMENT AND FISH SAMPLES BY GAS-CHROMATOGRAPHY MASS-SPECTROMETRY

被引：22
|
作者：
NISHIKAWA, Y
OKUMURA, T
机构：
[1] Environmental Pollution Control Center, Higashinari-ku, Osaka City, 537, 62-3, 1 Chome, Nakamichi
来源：
ANALYTICA CHIMICA ACTA | 1995年 / 312卷 / 01期
关键词：
GAS CHROMATOGRAPHY MASS SPECTROMETRY; NITROBENZENES; ENVIRONMENTAL ANALYSIS; WATERS; FISH; SEDIMENTS; RIVER WATER;
D O I：
10.1016/0003-2670(95)00201-A
中图分类号：
O65 [分析化学];
学科分类号：
070302 ; 081704 ;
摘要：
Traces of 10 nitrobenzenes in environmental samples such as river water, sediment and fish were determined by capillary gas chromatography-mass spectrometry (GC-MS) involving liquid-liquid extraction, steam distillation and column clean up procedures. The nitrobenzenes could be determined in water within the range 0.3-0.9 ng/ml with relative standard deviations (R.S.D.s) of 1.0-6.9%. The detection limits of the nitrobenzenes in water, sediment and fish samples were 0.12-0.23 ng/ml, 1.9-10.9 ng/g and 2.0-8.1 ng/g, respectively. Their recoveries from river water, sea water, sediment and fish samples were 86-133%, 87-133%, 87-111% and 61-137% with R.S.D.s of 1.3-3.8%, 0.3-3.8%, 2.4-12.5% and 2.0-16.9%, respectively.
引用
收藏
页码：45 / 55
页数：11
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