The synthesis of nanocrystalline nickel boride powders by ball milling of elemental components

被引：26

作者：

Corrias, A ^{[1
]}

Ennas, G ^{[1
]}

Marongiu, G ^{[1
]}

Musinu, A ^{[1
]}

Paschina, G ^{[1
]}

Zedda, D ^{[1
]}

机构：

[1] UNIV CAGLIARI,DIPARTIMENTO SCI CHIM,I-09124 CAGLIARI,ITALY

来源：

MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING | 1995年 / 204卷 / 1-2期

关键词：

synthesis; nickel boride powders; ball milling;

D O I：

10.1016/0921-5093(95)09963-8

中图分类号：

TB3 [工程材料学];

学科分类号：

0805 ; 080502 ;

摘要：

Solid state reaction induced by ball milling the elemental components has been investigated on Ni60B40 and Ni80B20 mixtures by means of transmission electron microscopy, X-ray diffraction and differential scanning calorimetry. The time evolution of the reaction is similar in the two samples, although slower in Ni80B20. Reaction begins with the formation of o-Ni3B and of a disordered phase. The final products are nanocrystalline o-Ni3B and unreacted nickel in Ni80B20 and nanocrystalline t-Ni2B in Ni60B40. Different milling conditions, tested on the Ni60B40 sample, do not modify the path but affect the rate of the solid state reaction.

引用

页码：211 / 216

页数：6

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