REACTION OF DIPHENYL(VINYL)PHOSPHINE WITH CARBONYLS [RU-3(CO)12] OR[OS-3(CO)12] - OXIDATIVE ADDITION AT [RU-3(CO)12] - SPECTROSCOPIC CHARACTERIZATION AND CRYSTAL-STRUCTURE OF [RU3(MU-H)(CO)8(PH2PCH=CH2)(MU-3-PH2PCH=CH)]

被引：17

作者：

GOBETTO, R

SAPPA, E

TIRIPICCHIO, A

CAMELLINI, MT

MAYS, MJ

机构：

[1] UNIV TURIN,DIPARTIMENTO CHIM INORGAN CHIM FIS & CHIM MAT,VIA PIETRO GIURIA 7,I-10125 TURIN,ITALY

[2] UNIV PARMA,IST CHIM GEN & INORGAN,CTR STUDIO STRUTTURIST DIFFRATTOMETR,CNR,I-43100 PARMA,ITALY

[3] UNIV CAMBRIDGE,CHEM LAB,CAMBRIDGE CB2 1EW,ENGLAND

来源：

JOURNAL OF THE CHEMICAL SOCIETY-DALTON TRANSACTIONS | 1990年 / 03期

关键词：

D O I：

10.1039/dt9900000807

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

引用

页码：807 / 811

页数：5

共 50 条

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[2] SYNTHESIS AND CRYSTAL-STRUCTURE OF [RU2(CO)6(MU-PPH2)(MU-PCH=CHC6H4)], A COMPLEX WITH AN UNPRECEDENTED PHOSPHA-BICYCLIC LIGAND, OBTAINED FROM [RU3(MU-H)(CO)8(PH2PCH=CH2)(MU-3-PH2PCH=CH)] VIA REDUCTIVE ELIMINATION-REACTIONS
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[J]. JOURNAL OF THE CHEMICAL SOCIETY-DALTON TRANSACTIONS, 1990, (02): : 703 - 705
[3] INTRAMOLECULAR AND INTERMOLECULAR BONDING IN RU-3(CO)(12), RU-3(CO)(9)(MU(3)ETA(2)ETA(2)-C6H6), AND RU-3(CO)(6)(MU-CO)(3)(MU(3)-S3C3H6)
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[J]. ORGANOMETALLICS, 1995, 14 (04) : 1992 - 2001
[4] THE REACTION OF PHSR(R=FC OR PH) WITH RU-3(CO)(12)
CULLEN, WR
RETTIG, SJ
ZHENG, TC
[J]. POLYHEDRON, 1995, 14 (19) : 2653 - 2661
[5] Synthesis and characterisation of diphenylvinylphosphine-substituted osmium and ruthenium carbonyl clusters; Crystal and molecular structures of [Os-3(CO)(11)(Ph(2)PCH=CH2)] and [Os-3(mu-H)(CO)(9)(mu-Ph(2)PCH=CH)]
Johnson, BFG
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[J]. JOURNAL OF THE CHEMICAL SOCIETY-DALTON TRANSACTIONS, 1996, (19): : 3825 - 3831
[6] A NEW FORM OF FLUXIONAL PROCESS IN THE STERICALLY HINDERED OXO CLUSTER [RU-3(MU(3)-O)(MU(3)-CO)(CO)(3)(MU-PH(2)PCH(2)PPH(2))(3)]
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[J]. INORGANIC CHEMISTRY, 1995, 34 (16) : 4239 - 4243
[7] The oxidative addition of a vinylic C-H bond of divinyl(phenyl)phosphine at M3(CO)12 carbonyls (M = Ru, Os).: Stepwise formation and crystal structure of [(μ-H)Ru3(CO)8{PPh(CH=CH2)2}{μ3-PPh(CH=CH2)(CH=CH)}]
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[J]. JOURNAL OF ORGANOMETALLIC CHEMISTRY, 1997, 547 (01) : 49 - 54
[8] Reactions of [Ru-3(CO)(10)(mu-Ph(2)PCH(2)PPh(2))] with secondary phosphines R(2)PH involving bulky substituents (R =(t)Bu, 1-Ad, Cy); X-ray crystal structures of [Ru-3(CO)(6)(mu-H)(2)(mu-PCy(2))(2)(mu-Ph(2)PCH(2)PPh(2))] and the electron-deficient carbonyl cluster [Ru-3(mu-CO)(CO)(4)(mu(3)-H)(mu-H)(mu P(t)Bu(2))(2)(mu-Ph(2)PCH(2)PPh(2))]
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[J]. JOURNAL OF ORGANOMETALLIC CHEMISTRY, 1996, 520 (1-2) : 15 - 22
[9] INTERACTION OF (MU-H)4RU4(CO)12 WITH DIPHOSPHINES IN THE PRESENCE OF TRIMETHYLAMINE N-OXIDE - X-RAY CRYSTAL-STRUCTURE ANALYSES OF (MU-H)4RU4(CO)10(MU-(PH2P(CH2)NPPH2))(N= 1,3,4), (MU-H)4RU4(CO)10(MU-(PH2PCH2(CH(CH3)PPH2)), AND (MU-H)4RU4(CO)10((PH2PCH2CH(CH3)PPH2))
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[J]. INORGANIC CHEMISTRY, 1987, 26 (06) : 867 - 874
[10] STRUCTURAL STUDIES ON RUTHENIUM CARBONYL HYDRIDES .13. SYNTHESIS OF (MU-H)3RU3(MU-3-CSET)(CO)9 AND ITS REARRANGEMENT TO (MU-H)RU3(MU-3-ETA-2-CH2SET)(CO)9 - CRYSTAL-STRUCTURE OF (MU-H)RU3(MU-3-ETA-2-CH2SET)(CO)9
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[J]. ORGANOMETALLICS, 1987, 6 (04) : 806 - 812

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