THE IDENTIFICATION OF NITROMETHAQUALONE AND ITS DIFFERENTIATION FROM SOME POSITIONAL ISOMERS

被引：0
|
作者：
CLARK, CC
机构：
来源：
JOURNAL OF FORENSIC SCIENCES | 1988年 / 33卷 / 04期
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暂无
中图分类号：
DF [法律]; D9 [法律]; R [医药、卫生];
学科分类号：
0301 ; 10 ;
摘要：
Nitromethaqualione [2-methyl-3(2''-methoxy-4" nitrophenyl)-4(3H)-guinazolinone] and its three positional isomers formed by moving the nitro group on the phenyl ring containing the 2''-methoxyl group have been synthesized and characterized. Mass spectra, infrared spectra, nuclear magnetic resonance spectra, and the gas-liquid chrmoatographic behavior of these compounds are presented. It is shown that infrared spectroscopy, nuclear magnetic resonance spectroscopy, and electron impact mass spectroscopy combined with gas-liqid chromatography are capable of differentiating nitromethaqualone from any of the studied isomers, methaqualone, and mecloqualone.
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页码：1035 / 1044
页数：10
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