SYNTHESIS AND CHARACTERIZATION OF CATIONIC TECHNETIUM COMPLEXES OF 1,2-BIS(DIMETHYLPHOSPHINO)ETHANE (DMPE) - STRUCTURE DETERMINATIONS OF TRANS-[TC-V(DMPE)2(OH)(O)](F3CSO3)2, TRANS-[TC-III(DMPE)2CL2]F3CSO3, AND [TC-I(DMPE)3]+ USING X-RAY-DIFFRACTION, EXAFS, AND TC-99 NMR

被引：103

作者：

VANDERHEYDEN, JL ^{[1
]}

KETRING, AR ^{[1
]}

LIBSON, K ^{[1
]}

HEEG, MJ ^{[1
]}

ROECKER, L ^{[1
]}

MOTZ, P ^{[1
]}

WHITTLE, R ^{[1
]}

ELDER, RC ^{[1
]}

DEUTSCH, E ^{[1
]}

机构：

[1] UNIV CINCINNATI,DEPT CHEM,CINCINNATI,OH 45221

来源：

INORGANIC CHEMISTRY | 1984年 / 23卷 / 20期

关键词：

D O I：

10.1021/ic00188a031

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

引用

页码：3184 / 3191

页数：8

共 21 条

[1] Photophysics and Luminescence Spectroelectrochemistry of [Tc(dmpe)3]+/2+ (dmpe=1,2-bis(dimethylphosphino)ethane)
Chatterjee, Sayandev
Del Negro, Andrew S.
Smith, Frances N.
Wang, Zheming
Hightower, Sean E.
Sullivan, B. Patrick
Heineman, William R.
Seliskar, Carl J.
Bryan, Samuel A.
JOURNAL OF PHYSICAL CHEMISTRY A, 2013, 117 (48): : 12749 - 12758
[2] COMPARISON OF THE CHEMICAL AND BIOLOGICAL PROPERTIES OF TRANS-[TC(DMPE)2CL2]+ AND TRANS-[RE(DMPE)2CL2]+, WHERE DMPE =1,2-BIS(DIMETHYLPHOSPHINO)ETHANE - SINGLE-CRYSTAL STRUCTURAL-ANALYSIS OF TRANS-[RE(DMPE)2CL2]PF6
VANDERHEYDEN, JL
HEEG, MJ
DEUTSCH, E
INORGANIC CHEMISTRY, 1985, 24 (11) : 1666 - 1673
[3] THIOLATO TECHNETIUM COMPLEXES .2. SYNTHESIS, CHARACTERIZATION, ELECTROCHEMISTRY, AND SPECTROELECTROCHEMISTRY OF THE TECHNETIUM(III) COMPLEXES TRANS-[TC(SR)2(DMPE)2]+, WHERE R IS AN ALKYL OR BENZYL GROUP AND DMPE IS 1,2-BIS(DIMETHYLPHOSPHINO)ETHANE
KONNO, T
KIRCHHOFF, JR
HEINEMAN, WR
DEUTSCH, E
INORGANIC CHEMISTRY, 1989, 28 (06) : 1174 - 1179
[4] ELECTRON-TRANSFER REACTIONS OF TECHNETIUM AND RHENIUM COMPLEXES .3. PULSE-RADIOLYSIS STUDIES ON TRANS-[MIIIX2(DMPE)2]+ AND [MI(DMPE)3]+ COMPLEXES IN AQUEOUS AND AQUEOUS SURFACTANT MEDIA, WHERE M = TC OR RE, X = CL OR BR, AND DMPE = 1,2-BIS(DIMETHYLPHOSPHINO)ETHANE
ROODT, A
SULLIVAN, JC
MEISEL, D
DEUTSCH, E
INORGANIC CHEMISTRY, 1991, 30 (24) : 4545 - 4549
[5] ELECTRON-TRANSFER REACTIONS OF TECHNETIUM COMPLEXES .1. RATE OF THE SELF-EXCHANGE REACTION OF THE TC(I)/TC(II) COUPLE [TC(DMPE)3]+/2+, WHERE DMPE = 1,2-BIS(DIMETHYLPHOSPHINO)ETHANE
DOYLE, MN
LIBSON, K
WOODS, M
SULLIVAN, JC
DEUTSCH, E
INORGANIC CHEMISTRY, 1986, 25 (19) : 3367 - 3371
[6] Solid state study on rhenium dimethylphosphinoethane complexes:: X-ray crystal structures of trans-[ReO2(dmpe)2]PF6•2H2O, trans-[ReO(OH)(dmpe)2](CF3SO3)2, trans-[ReN(Cl)(dmpe)2]CF3SO3 and trans-[ReCl2(dmpe)2]ReO4
Engelbrecht, HP
Jurisson, SS
Cutler, CS
den Drijver, L
Roodt, A
SYNTHESIS AND REACTIVITY IN INORGANIC METAL-ORGANIC AND NANO-METAL CHEMISTRY, 2005, 35 (01) : 83 - 99
[7] Luminescence-Based Spectroelectrochemical Sensor for [Tc(dmpe)3]2+/+ (dmpe=1,2-bis(dimethylphosphino)ethane) within a Charge-Selective Polymer Film
Chatterjee, Sayandev
Del Negro, Andrew S.
Edwards, Matthew K.
Bryan, Samuel A.
Kaval, Necati
Pantelic, Nebojsa
Morris, Laura K.
Heineman, William R.
Seliskar, Carl J.
ANALYTICAL CHEMISTRY, 2011, 83 (05) : 1766 - 1772
[8] THE CHEMISTRY OF CHROMIUM NITRILE COMPLEXES OF 1,2-BIS(DIMETHYLPHOSPHINO)-ETHANE - X-RAY CRYSTAL-STRUCTURES OF TRANS-[CRIVCL(NET)(DMPE)2]CF3SO3, TRANS-[CRIV(N=CHME)2(DMPE)2][BPH4]2, AND TRANS-[CO0(H.NCME)2(DMPE)2][BPH4]2
BARRON, AR
SALT, JE
WILKINSON, G
MOTEVALLI, M
HURSTHOUSE, MB
JOURNAL OF THE CHEMICAL SOCIETY-DALTON TRANSACTIONS, 1987, (12): : 2947 - 2954
[9] REACTIONS OF BIS[1,2-BIS(DIMETHYLPHOSPHINO)ETHANE]BIS(DINITROGEN)CHROMIUM(0) AND BIS(CARBONYL)CHROMIUM(0) WITH ACIDS AND OXIDIZING-AGENTS - X-RAY CRYSTAL-STRUCTURES OF TRANS-CR11(O2CCF3)2(DMPE)2,TRANS-[CR11(CNR)2(DMPE)2][CF3SO3]2(R=ME OR ET), "TRANS-[CR111CL2(DMPE)2]BPH4.CH2CL2, TRANS-[CR1(CO)2(DMPE)2]BPH4, AND [CR0H(CO)2(DMPE)2]BPHS
SALT, JE
WILKINSON, G
MOTEVALLI, M
HURSTHOUSE, MB
JOURNAL OF THE CHEMICAL SOCIETY-DALTON TRANSACTIONS, 1986, (06): : 1141 - 1154
[10] PREPARATION AND CHARACTERIZATION OF RHODIUM(III) COMPLEXES CONTAINING (2-AMINOETHYL)DIMETHYLPHOSPHINE (EDMP) OR 1,2-BIS(DIMETHYLPHOSPHINO)ETHANE (DMPE). STRUCTURES OF FAC-[RH(EDMP)3]3+, TRANS(CL,CL),CIS(P,P)-[RHCL2(EDMP)2]+, AND TRANS-[RHCL2(DMPE)2]+
SIMONSEN, KP
SUZUKI, N
HAMADA, M
KOJIMA, M
OHBA, SG
SAITO, YH
FUJITA, J
BULLETIN OF THE CHEMICAL SOCIETY OF JAPAN, 1989, 62 (12) : 3790 - 3800

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