CRYSTAL-STRUCTURE OF MU-OXO-BIS[OXO-SALICYLALDEHYDBENZOYLHYDRAZONATO(2-)]VANADIUM(V)

被引：0

作者：

SUNDHEIM, A ^{[1
]}

MATTES, R ^{[1
]}

机构：

[1] WESTFAL WILHELMS UNIV,INST ANORGAN CHEM,D-48149 MUNSTER,GERMANY

来源：

ZEITSCHRIFT FUR NATURFORSCHUNG SECTION B-A JOURNAL OF CHEMICAL SCIENCES | 1993年 / 48卷 / 12期

关键词：

VANADIUM(V) COMPLEXES; SCHIFFBASE COMPLEXES; CRYSTAL STRUCTURE;

D O I：

暂无

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

The dimeric title complex contains a V2O34+ unit with a rather small (112.6 degrees) V-O-V angle and exhibits crystallographic C-2 symmetry. Each vanadium center is equatorially coordinated by the tridentate doubly deprotonated hydrazone formed from salicylaldehyde and benzoylhydrazine. The coordination sphere is distorted square pyramidal. Crystal data: orthorhombic, space group Pnc 2, a = 758.2(2), b = 1454.4(3), c = 1186.1(2) pm, Z = 4, 1137 reflections, 184 parameters, R (R(w)) = 0.032 (0.032).

引用

页码：1848 / 1850

页数：3

共 50 条

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