DETERMINATION OF LEAD IN SOIL BY SLURRY ELECTROTHERMAL ATOMIC-ABSORPTION SPECTROMETRY WITH A FAST TEMPERATURE PROGRAM

被引:30
|
作者
HINDS, MW
LATIMER, KE
JACKSON, KW
机构
[1] UNIV SASKATCHEWAN,DEPT CHEM,SASKATOON S7N 0W0,SASKATCHEWAN,CANADA
[2] SUNY ALBANY,NEW YORK STATE DEPT HLTH,WADSWORTH CTR LABS,ALBANY,NY 12201
[3] SUNY ALBANY,SCH PUBL HLTH,ALBANY,NY 12201
关键词
ELECTROTHERMAL ATOMIC ABSORPTION SPECTROMETRY; SLURRY; FAST TEMPERATURE PROGRAM; SOIL ANALYSIS;
D O I
10.1039/ja9910600473
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
A fast temperature programme for the determination of Pb in soil by slurry-electrothermal atomic absorption spectrometry was developed by omitting the charring step and drying at a higher temperature for a shorter time. The effects of drying temperature and time were systematically studied. Work with phosphate and Mg-Pd as chemical modifiers indicates that better results can be obtained without the use of modifiers.
引用
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页码:473 / 476
页数:4
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