PREPARATIVE-SCALE SUPERCRITICAL-FLUID CHROMATOGRAPHY

被引:19
|
作者
BARTLE, KD
BEVAN, CD
CLIFFORD, AA
JAFAR, SA
MALAK, N
VERRALL, MS
机构
[1] UNIV LEEDS,SCH CHEM,LEEDS LS2 9JT,W YORKSHIRE,ENGLAND
[2] GLAXO GRP RES LTD,GREENFORD UB6 0HE,MIDDX,ENGLAND
[3] SMITHKLINE BEECHAM PHARMACEUT,BROCKHAM PK RES CTR,BETCHWORTH RH3 7AJ,SURREY,ENGLAND
基金
英国工程与自然科学研究理事会;
关键词
D O I
10.1016/0021-9673(94)01058-M
中图分类号
Q5 [生物化学];
学科分类号
071010 ; 081704 ;
摘要
An apparatus for the study of preparative supercritical fluid chromatography (SFC) has been built and used to study the separation of a model system [a 1:1 (w/w) mixture of fluorene and phenanthrene] and a more real system (a mixture of milbemycins containing also other extracted material). The principles of preparative SFC are given and applied to these studies, and some conclusions about the optimisation of preparative SFC drawn.
引用
收藏
页码:579 / 585
页数:7
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