DETERMINATION OF DIMETHYL SULFIDE IN BLOOD AND ADIPOSE-TISSUE BY HEADSPACE GAS-ANALYSIS

被引：6
|
作者：
TERAZAWA, K [1 ]
KAJI, H [1 ]
AKABANE, H [1 ]
TAKATORI, T [1 ]
机构：
[1] IWAMIZAWA ROSAI HOSP,HLTH EXAMINAT CTR,IWAMIZAWA 068,JAPAN
来源：
JOURNAL OF CHROMATOGRAPHY-BIOMEDICAL APPLICATIONS | 1991年 / 565卷 / 1-2期
关键词：
D O I：
10.1016/0378-4347(91)80409-6
中图分类号：
O65 [分析化学];
学科分类号：
070302 ; 081704 ;
摘要：
A method for the headspace analysis of dimethyl sulphide in blood and adipose tissue has been established. Blood (0.2 ml) or adipose tissue (0.5 g) with added dimethyl sulphide was sealed in a 10-ml vial using PTFE sheet to prevent escape of dimethyl sulphide from the headspace. Equilibration was performed at 60-degrees-C for 4 h, and 20-mu-l of gaseous phase sampled from the headspace was subjected to gas chromatography (with flame photometric detection). Calibration curves were prepared for the two samples. Linearity was observed in the range from 5-10-mu-g to 2 mg.
引用
收藏
页码：453 / 456
页数：4
相关论文
共 50 条
  • [1] HEADSPACE GAS-ANALYSIS BY GAS-CHROMATOGRAPHY
    DROZD, J
    NOVAK, J
    JOURNAL OF CHROMATOGRAPHY, 1979, 165 (02): : 141 - 165
  • [2] Nonlinear standard addition method in the determination of dimethyl sulfide in beer by headspace gas chromatography
    Wu, ZY
    Zhou, JK
    ANALYTICAL LETTERS, 1999, 32 (13) : 2691 - 2701
  • [3] Dimethyl sulfide precursor in malt by headspace gas chromatography
    Bartnett, C
    Attard, P
    Bresler, S
    daCosta, PCR
    Dupire, S
    Eikens, D
    Laycock, G
    Loran, C
    Oxford, E
    Schwarz, P
    Shelton, I
    Stenroos, L
    VeldhuijzenDoorduin, R
    Wheeler, J
    Yoshimura, N
    Munar, M
    JOURNAL OF THE AMERICAN SOCIETY OF BREWING CHEMISTS, 1996, 54 (04) : 252 - 253
  • [4] Dimethyl sulfide precursor in malt by headspace gas chromatography
    Bartnett, C
    Attard, P
    Benard, M
    Bresler, S
    Garcia, MC
    Haag, R
    Laycock, G
    Lorenzana, R
    Oxford, E
    Penarski, J
    Perez, G
    Rasmussen, H
    Shamaila, M
    Shelton, I
    Stenroos, L
    Yoshimura, N
    Munar, M
    JOURNAL OF THE AMERICAN SOCIETY OF BREWING CHEMISTS, 1997, 55 (04) : 205 - 206
  • [5] THE DETERMINATION OF DIMETHYL SULFIDE IN BEER BY HEADSPACE GAS-CHROMATOGRAPHY - A COLLABORATIVE INVESTIGATION OF PRECISION
    MUNDY, AP
    JOURNAL OF THE INSTITUTE OF BREWING, 1991, 97 (01) : 45 - 46
  • [6] GAS-LIQUID-CHROMATOGRAPHIC DETERMINATION OF HEXESTROL RESIDUES IN ADIPOSE-TISSUE
    TOBIOKA, H
    KAWASHIMA, R
    JOURNAL OF THE ASSOCIATION OF OFFICIAL ANALYTICAL CHEMISTS, 1981, 64 (03): : 709 - 713
  • [7] HEADSPACE GAS-ANALYSIS AS A MEASURE OF RANCIDITY IN CORN CHIPS
    ROBARDS, K
    KERR, AF
    PATSALIDES, E
    KORTH, J
    JOURNAL OF THE AMERICAN OIL CHEMISTS SOCIETY, 1988, 65 (10) : 1621 - 1626
  • [8] DETERMINATION OF PROTEIN IN ADIPOSE-TISSUE EXTRACTS
    TORNQVIST, H
    BELFRAGE, P
    JOURNAL OF LIPID RESEARCH, 1976, 17 (05) : 542 - 545
  • [9] BLOOD-CIRCULATION IN ADIPOSE-TISSUE
    ROSELL, S
    BELFRAGE, E
    PHYSIOLOGICAL REVIEWS, 1979, 59 (04) : 1078 - 1104
  • [10] DIMETHYL SULFIDE PRECURSOR IN MALT BY HEADSPACE GAS-CHROMATOGRAPHY
    DUNCOMBE, D
    BARTNETT, C
    CERWINKA, M
    EIKENS, D
    DRUMMOND, C
    HURTEAU, P
    VELDHUYZENDOORDUIN, R
    YOSHIMURA, N
    CRUMPLEN, R
    JOURNAL OF THE AMERICAN SOCIETY OF BREWING CHEMISTS, 1994, 52 (04) : 193 - 193
12345