THE SYNTHESIS OF NOVEL POLYCYCLIC HETEROCYCLIC RING-SYSTEMS VIA PHOTOCYCLIZATION .10. SYNTHESIS AND STRUCTURE DETERMINATION OF NAPHTHO[1',2'-4,5]THIENO[3,2-A]-4,7-PHENANTHROLINE

被引：23

作者：

MUSMAR, MJ ^{[1
]}

ZEKTZER, AS ^{[1
]}

CASTLE, RN ^{[1
]}

DALLEY, NK ^{[1
]}

机构：

[1] BRIGHAM YOUNG UNIV,DEPT CHEM,PROVO,UT 84602

来源：

JOURNAL OF HETEROCYCLIC CHEMISTRY | 1993年 / 30卷 / 02期

关键词：

D O I：

10.1002/jhet.5570300235

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

Naphtho[1',2':4,5]thieno[3,2-a]-4,7-phenanthroline, a novel hexacyclic ring system has been synthesized in four steps. The H-1 and C-13 nmr assignments have been made using two-dimensional nmr techniques. The tertiary helical structure was determined by X-ray crystallographic analysis.

引用

页码：487 / 492

页数：6

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