Synthesis of MnxZn(1−x)Fe2O4 nanoparticles by ball-milling hydrothermal method

被引:0
|
作者
Zhenyu Lai
Guangliang Xu
Min Liu
A Ahniyaz
M Yoshimura
机构
[1] Southwest University of Science and Technology,Key Laboratory of Advanced Building Materials of Sichuan Province
[2] Tokyo Institute of Technology,Materials and Structures Laboratory
关键词
Mn; Zn; Fe; O; nanoparticles; ball milling; hydrothermal;
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学科分类号
摘要
SMnxZn1−xFe2O4 (x=1,0.9,0.8,0.7,0.6,0.5,0.25,0) nanoparticles were prepared by ball-milling hydrothermal and investigated by X-ray diffraction, DTG and TEM. Nanocrystallite grain size was determined by X-ray linewidth to be from 63 Å to 274 Å. The thermal properties indicate absorbed water still remain at low temperature, crystalline wate will be decomposed from 230 °C to 260 °C, partial Mn2+ will be oxidized near 730 °C. TEM shows the ferrite particles pocess a spherical morphology and uniform nanosize.
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页码:151 / 154
页数:3
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