Current Status of AIST X-ray-Absorption-Spectroscopy (XAFS) Instrument with 100-Pixel Superconducting-Tunnel-Junction Array Detector

被引:0
|
作者
S. Shiki
M. Ukibe
N. Matsubayashi
N. Zen
M. Koike
Y. Kitajima
M. Ohkubo
机构
[1] National Institute of Advanced Industrial Science and Technology (AIST),
[2] High Energy Accelerator Research Organization (KEK),undefined
来源
关键词
XAS; XAFS; X-ray absorption spectroscopy; X-ray absorption fine structure; Superconducting tunnel junction; X-ray detector; Materials analysis;
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学科分类号
摘要
We constructed a fluorescence yield X-ray absorption fine structure (XAFS) apparatus for the measurement of local structure around trace light element impurities in light element matrices. Our XAFS instrument with a 100-pixel STJ detector is now in the stage of routine operation and open to users at a synchrotron radiation facility (KEK PF). The average energy resolution of the 100 pixels is 11.8 ±\documentclass[12pt]{minimal} \usepackage{amsmath} \usepackage{wasysym} \usepackage{amsfonts} \usepackage{amssymb} \usepackage{amsbsy} \usepackage{mathrsfs} \usepackage{upgreek} \setlength{\oddsidemargin}{-69pt} \begin{document}$$\pm $$\end{document} 0.6 at 400 eV in a sensitive area of 1 mm2\documentclass[12pt]{minimal} \usepackage{amsmath} \usepackage{wasysym} \usepackage{amsfonts} \usepackage{amssymb} \usepackage{amsbsy} \usepackage{mathrsfs} \usepackage{upgreek} \setlength{\oddsidemargin}{-69pt} \begin{document}$$^{2}$$\end{document}. As an example of functional materials, we successfully measured nitrogen K-edge XAFS spectra of a compound semiconductor, 4H-SiC, with a nitrogen dopant concentration of 300 ppm. The faint N-K line was clearly separated from the strong C-K line.
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页码:604 / 609
页数:5
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