Silver(I) Compounds with Perfluorinated Aromatic Thiols C6F5C6F4SH, C10F7SH, and C6F5SH as Precursors for Silver Nanoparticles

被引：0
|
作者：
S. V. Larionov
T. G. Leonova
N. I. Batrachenko
I. V. Korol’kov
V. S. Danilovich
V. E. Platonov
A. M. Maksimov
V. P. Fadeeva
机构：
[1] Russian Academy of Sciences,Nikolaev Institute of Inorganic Chemistry, Siberian Branch
[2] Russian Academy of Sciences,Vorozhtsov Novosibirsk Institute of Organic Chemistry, Siberian Branch
来源：
Russian Journal of Inorganic Chemistry | 2008年 / 53卷
关键词：
Thermolysis; Thiophenol; Thermolysis Product; Coherent Domain Size; Initial Sample Weight;
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摘要：
Silver(I) compounds with perfluorinated aromatic thiols (4-nonafluorodiphenylthiol C6F5C6F4SH (HL1), 2-heptafluoronaphthalenethiol C10F7SH (HL2), and pentafluorothiophenol C6F5SH (HL3), namely AgL1 (I), AgL2 (II), AgL3 (III), were prepared. The thermal properties of compounds I–III and the composition of thermolysis products were studied. By powder X-ray diffraction and electron microscopy, it was shown that thermolysis of compounds I–III under argon and thermolysis of compound III in air yield Ag nanoparticles.
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页码：209 / 212
页数：3
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