Characterization of zinc and zinc cyanide nanoparticles in carbon matrices prepared by solid-phase pyrolysis of zinc-phthalocyanine

被引：0

作者：

A. A. Mirzakhanyan

A. S. Manukyan

H. T. Gyulasaryan

A. K. Ginoyan

M. Kh. Nurijanyan

Yu. I. Yuzyuk

E. Yu. Kaniukov

E. G. Sharoyan

机构：

[1] NAS of Armenia,Institute for Physical Research

[2] Southern Federal University,Division of Cryogenic Research, Scientific

[3] NAS of Belarus,Practical Materials Research Centre

来源：

Journal of Contemporary Physics (Armenian Academy of Sciences) | 2016年 / 51卷

关键词：

zinc and zinc cyanide nanoparticles; solid-phase pyrolysis; SEM images; size distribution; X-ray diffraction; Raman shift;

D O I：

暂无

中图分类号：

学科分类号：

摘要：

Using solid-phase pyrolysis of Zn-phthalocyanine (ZnC32H16N8), we have prepared zinc and zinc cyanide nanoparticles in carbon matrices with a zinc concentration of 3 at %. The structure and composition of samples were investigated by the methods of scanning electron microscopy, X-ray diffraction, and Raman spectroscopy. It is shown that at low pyrolysis temperature (700°C) only the Zn nanoparticles are formed, whereas at higher temperature (900°C) a certain amount of Zn(CN)2 nanoparticles are also synthesized. The mean diameter of nanoparticles is about 150 nm, and their size distribution has a logarithmically normal shape.

引用

页码：191 / 195

页数：4

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