Reaction of N,N′-bis(trimethylsilyl)dicyandiamide with bis(η5-cyclopentadienylvanadium) dichloride

被引：0
|
作者：
A. S. Gordetsov
S. V. Zimina
S. V. Saprykina
L. B. Loginova
A. V. Piskunov
V. F. Ur’yash
E. M. Moseeva
机构：
[1] Nizhnii Novgorod State Medical Academy,
来源：
Russian Journal of General Chemistry | 2011年 / 81卷
关键词：
Differential Thermal Analysis; General Chemistry; Melamin; Trimethylsilyl; Cyanamide;
D O I：
暂无
中图分类号：
学科分类号：
摘要：
1,3,5-Tris[bis(η5-cyclopentadienyl)chlorovanadium]melamin is prepared in high yield by the reaction of N,N′-bis(trimethylsilyl)dicyandiamide with bis(η5-cyclopentadienylvanadium) dichloride in tetrahydrofuran. As side products, trimethylchlorosilane and cyclopentadiene formed. Reaction of N,N′-bis(trimethylsilyl) dicyandiamide with benzoyl chloride results in the formation of tris(benzoyl)melamin.
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页码：658 / 662
页数：4
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