Synthesis of acetylated glycosyl-containing thiourea derivatives based on the alkaloids cytisine and anabasine and the molecular structure of N-cytisino-N′-(2,3,4,6-tetraO-acetyl-β-D-glucopyranosyl)thiocarbamide

被引：0

作者：

I. V. Kulakov

O. A. Nurkenov

A. E. Arinova

D. M. Turdybekov

S. A. Talipov

B. T. Ibragimov

机构：

[1] Institute of Organic Synthesis and Carbon Chemistry of the Republic of Kazakhstan,A. S. Sadykov Institute of Bioorganic Chemistry

[2] Multi-discipline Humanitarian-Technical University,undefined

[3] Academy of Sciences of the Republic of Uzbekistan,undefined

来源：

Chemistry of Natural Compounds | 2011年 / 47卷

关键词：

cytisine; anabasine; glycosylisothiocyanate; x-ray crystal structure analysis;

D O I：

暂无

中图分类号：

学科分类号：

摘要：

Glycosylthiourea derivatives were synthesized from the alkaloids cytisine and anabasine and 1-deoxy-2,3,4,6tetra-O-acetyl-β-D-glucopyranosylisothiocyanate. The structures of the synthesized compounds were proved using PMR spectroscopy, mass spectrometry, and an x-ray crystal structure analysis.

引用

页码：777 / 780

页数：3

共 12 条

[1] SYNTHESIS OF ACETYLATED GLYCOSYL-CONTAINING THIOUREA DERIVATIVES BASED ON THE ALKALOIDS CYTISINE AND ANABASINE AND THE MOLECULAR STRUCTURE OF N-CYTISINO-N′-(2,3,4,6-TETRA-O-ACETYL-β-D-GLUCOPYRANOSYL)THIOCARBAMIDE
Kulakov, I. V.
Nurkenov, O. A.
Arinova, A. E.
Turdybekov, D. M.
Talipov, S. A.
Ibragimov, B. T.
CHEMISTRY OF NATURAL COMPOUNDS, 2011, 47 (05) : 777 - 780
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[3] Synthesis and characterization of N-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-thiocarbamic-4-hydroxy-benzoyl hydrazine dihydrate
Zhang, SS
Ye, SJ
Li, XM
Gu, SS
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[4] Synthesis and characterization of N-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl) thiocarbamic 2,4-dihydroxy benzoyl hydrazine monohydrate
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Ye, SJ
Tang, XL
Ding, CF
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Xiao, HL
Sun, PP
Zhao, PS
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[6] Synthesis, anticancer activity, and molecular simulation of N-(2,3,4,6-tetra-O-acetyl-β-<sc>d</sc>-glucopyranosyl)thioureas containing a pyrimidine ring
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Thanh, Nguyen Dinh
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NEW JOURNAL OF CHEMISTRY, 2024, 48 (20) : 9208 - 9223
[7] Synthesis, Crystal Structure and Spectrometry Study of Chiral N-Ethyl-N'-(2',3',4',6'-tetra-O-acetyl-β-D-glycosyl)-thiocarbamide
JIAN Fang-Fang② XIAO Hai-Lian SUN Ping-Ping (New Materials & Function Coordination Chemistry Laboratory
结构化学, 2003, (05) : 564 - 568
[8] STRUCTURE AND REACTIVITY OF GLYCOSIDES .2. SYNTHESIS AND STRUCTURE OF O-ARYL-N-(2,3,4,6-TETRA-O-ACETYL-BETA-D-GLUCOPYRANOSYL)THIOCARBAMATES
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[9] Synthesis and evaluation of in vivo antioxidant, in vitro antibacterial, MRSA and antifungal activity of novel substituted isatin N-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)thiosemicarbazones
Nguyen Dinh Thanh
Nguyen Thi Kim Giang
Tran Ha Quyen
Doan Thi Huong
Vu Ngoc Toan
EUROPEAN JOURNAL OF MEDICINAL CHEMISTRY, 2016, 123 : 532 - 543
[10] 2,3,4,6-tetra-O-Acetyl-D-Gluconic Acid: Crystal Structure and Application in the Synthesis of N-(D-gluconyl) Derivatives of D-Glucosamine
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Myszka, Henryk
Cyman, Magdalena
Grzywacz, Daria
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JOURNAL OF CARBOHYDRATE CHEMISTRY, 2014, 33 (01) : 33 - 47

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