Synthesis of High Dispersion and Uniform Nano-sized Flame Retardant-Used Hexagonal Mg(OH)2

被引:0
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作者
Luyao Zong
Liyan Li
Jiyi Zhang
Xiaobo Yang
Gongxuan Lu
Zhicheng Tang
机构
[1] Chinese Academy of Sciences,State Key Laboratory for Oxo Synthesis and Selective Oxidation, National Engineering Research Center for Fine Petrochemical Intermediates, Lanzhou Institute of Chemical Physics
[2] Qinghai Salt Lake Industry Co.,Key Laboratory of Qinghai Salt Lake Resources Comprehensive Utilization
[3] Ltd.,School of Petroleum and Chemical
[4] Lanzhou University of Technology,Key Laboratory of Comprehensive and Highly Efficient Utilization of Salt Lake Resources, Qinghai Institute of Salt Lake
[5] Chinese Academy of Sciences,undefined
来源
关键词
Mg(OH); Flame retardant; Hydrothermal method; Hexagonal; High dispersion;
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中图分类号
学科分类号
摘要
Nanosized dispersive flake-like magnesium hydroxide (Mg(OH)2) had been prepared by a hydrothermal method. In the process, when the surfactant polyvinyl pyrrolidone was added, high dispersion, small particle size and large specific surface area of hexagonal crystal magnesium hydroxide was obtained by ultrasonic dispersion and temperature program. The flame retardant of Mg(OH)2 was systematically explored by scanning electron microscope (SEM), transmission electron microscopy, X-ray diffraction, BET analysis and thermo-gravimetric analysis tests. SEM showed the formation of uniform and small size magnesium hydroxide particle with hexagonal nanoscale. Under the optimized conditions, high nano-sized hexagonal Mg(OH)2 was acquired with a mean particle size of 134 nm and a specific surface area of 26.66 m2/g. According to TGA results, the sample’s decomposition temperature was 626.9 K, which was consistent with the reported literature. It is vitally prospected that the prepared hexagonal Mg(OH)2 is to be applied to the industry as a flame retardant.
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页码:1831 / 1841
页数:10
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