Reactions of 2-phenyl-4,4-bis(trifluoromethyl)-4,5-dihydro-1,3,2-benzodioxaphosphepin-5-one with phenanthrenequinone and dibenzoyl

被引：0
|
作者：
V. F. Mironov
L. M. Burnaeva
Yu. Yu. Borisova
A. T. Gubaidullin
I. A. Litvinov
G. A. Ivkova
I. V. Konovalova
机构：
[1] Russian Academy of Sciences,Arbuzov Institute of Organic and Physical Chemistry, Kazan Research Center
[2] Privolzhsk (Kazan) Federal University,undefined
来源：
Russian Journal of Organic Chemistry | 2011年 / 47卷
关键词：
Phosphite; Trifluoromethyl; Phosphorus Atom; Dibenzoyl; Phenanthrenequinone;
D O I：
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中图分类号：
学科分类号：
摘要：
Reactions of 2-phenyl-4,4-bis(trifluoromethyl)-4,5-dihydro-1,3,2-benzodioxaphosphepin-5-one with 9,10-phenanthrenequinone and dibenzoyl gave hydrolytically unstable spirophosphoranes with five- and seven-membered rings, 2-phenyl-4,4-bis(trifluoromethyl)-4,5-dihydrospiro[[1,3,2]benzodioxaphosphepine-2,2′-phenanthro[9,10-d][1,3,2]dioxaphosphol]-5-one and 2,4′,5′-triphenyl-4,4-bis(trifluoromethyl)-4,5-dihydrospiro[[1,3,2]benzodioxaphosphepine-2,2′-[1,3,2]dioxaphosphol]-5-one. The structure of the first of these was proved by X-ray analysis.
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页码：1521 / 1526
页数：5
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