Aqueous pretreatment for reactive ball milling of cellulose

被引：0
|
作者：
Pei Huang
Min Wu
Shigenori Kuga
Yong Huang
机构：
[1] Chinese Academy of Sciences,Institute of Chemistry
[2] Chinese Academy of Sciences,Technical Institute of Physics and Chemistry
[3] Chinese Academy of Sciences,Graduate School
[4] The University of Tokyo,Department of Biomaterials Science, Graduate School of Agricultural and Life Sciences
来源：
Cellulose | 2013年 / 20卷
关键词：
Cellulose nanofiber; Aqueous pretreatment; Reactive ball milling; Mechanochemistry;
D O I：
暂无
中图分类号：
学科分类号：
摘要：
Aqueous swelling pretreatment of cellulose was found highly effective for reactive ball milling to prepare surface-esterified cellulose nanofibers. Compared with starting from dry cellulose, water- or 2 % NaOH-pre-swollen materials were esterified and dispersed in significantly shorter milling time. Especially commercial kraft pulp was difficult to disperse even with water pretreatment, but 2 % NaOH treatment gave full surface esterification with a bulk degree of substitution of 0.69 by 12-h ball milling, presumably because of removal of non-cellulosic components.
引用
收藏
页码：2175 / 2178
页数：3
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