Crystal structure, thermal analysis, and IR spectrometric investigation of bis(tert-butylammonium) sulfate

被引：0
|
作者：
Taha Guerfel
Mohamed Bdiri
Amor Jouini
机构：
[1] Université du centre,Laboratoire de Chimie du Solide, Département de Chimie, Faculté des Sciences de Monastir
[2] Université du centre,Laboratoire de Chimie du Solide, Département de Chimie, Faculté des Sciences de Monastir
来源：
Journal of Chemical Crystallography | 2000年 / 30卷
关键词：
organic sulfate; crystal structure; DTA/TG/DSC; IR spectra;
D O I：
暂无
中图分类号：
学科分类号：
摘要：
Chemical preparation, X-ray single crystal, thermal analysis, and IR spectrometric investigation of (C4H12N)2SO4, denoted tBAS, are described. The compound crystallizes in the monoclinic system with C2/c space group. Its unit cell dimensions are a = 11.1585(5) Å, b = 6.2148(4) Å, c = 20.070(1) Å, β = 102.004(4)°, V = 1361.4(1) Å3, and Z = 4. The crystal structure of tBAS can be described as a typical thick layered organization built by all the components of the structure and centered by planes z = 1/4 and 3/4. Connection in these layers are established by N—H···O hydrogen bonds. Thermal analysis shows a reversible weak phase transition.
引用
收藏
页码：799 / 804
页数：5
相关论文
共 50 条
  • [1] Crystal structure, thermal analysis, and IR spectrometric investigation of bis(tert-butylammonium) sulfate
    Guerfel, T
    Bdiri, M
    Jouini, A
    JOURNAL OF CHEMICAL CRYSTALLOGRAPHY, 2000, 30 (12) : 799 - 804
  • [2] BIS(TERT-BUTYLAMMONIUM) MOLYBDATE(VI)
    ROMAN, P
    JOSE, AS
    LUQUE, A
    GUTIERREZZORRILLA, JM
    MARTINEZRIPOLL, M
    ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1994, 50 : 1189 - 1191
  • [3] Bis(diisopropylammonium) thiosulfate and bis(tert-butylammonium) thiosulfate
    Okuniewski, Andrzej
    Chojnacki, Jaroslaw
    Baranowska, Katarzyna
    Becker, Barbara
    ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 2013, 69 : 195 - +
  • [4] tert-butylammonium phosphomolybdates. Synthesis, crystal structure, thermal behaviour and electrochemical properties
    Wery, ASJ
    GutierrezZorrilla, JM
    Luque, A
    Ugalde, M
    Roman, P
    POLYHEDRON, 1997, 16 (15) : 2589 - 2597
  • [5] Crystal structure, thermal analysis and IR spectrometric investigation of bis (2-amino-6-methyl) pyridinium sulfate
    Guerfel, T
    Chtioui, A
    Gharbi, A
    Jouini, A
    CRYSTAL RESEARCH AND TECHNOLOGY, 2006, 41 (04) : 416 - 422
  • [6] STRUCTURE OF TERT-BUTYLAMMONIUM HEXACHLOROTELLURATE(IV)
    ISHIDA, H
    KASHINO, S
    ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1992, 48 : 1673 - 1675
  • [7] Influence of protonation on crystal packing and thermal behaviour of tert-butylammonium decavanadates
    Wery, ASJ
    GutierrezZorrila, JM
    Luque, A
    Roman, P
    MartinezRipoll, M
    POLYHEDRON, 1996, 15 (24) : 4555 - 4564
  • [8] Influence of protonation on crystal packing and thermal behaviour of tert-butylammonium decavanadates
    Wery, A. S. J.
    Gutierrez-Zorrila, J. M.
    Luque, A.
    Roman, P.
    Polyhedron, 15 (24):
  • [9] Crystal structure, thermal analysis and IR spectrometric investigation of L-tyrosine hydrazide sulfate
    Chtioui, A
    Guerfel, T
    Benhamada, L
    Jouini, A
    SOLID STATE SCIENCES, 2001, 3 (08) : 859 - 866
  • [10] tert-butylammonium silicododecamolybdate. Synthesis, vibrational study, crystal structure, thermal behaviour and electrochemical properties
    Wery, ASJ
    Gutierrez-Zorrilla, JM
    Luque, A
    Vitoria, P
    Roman, P
    Martinez-Ripoll, M
    POLYHEDRON, 1998, 17 (08) : 1247 - 1255
12345